Process for producing chloro-fatty acid methyl ester by utilizing biodiesel

A technology for chlorinated fatty acid methyl ester and biodiesel, which is applied in the fields of biofuel, carboxylate preparation, organic compound preparation, etc., can solve the problems of physiological toxicity residue, low flash point of finished products, and high freezing point, and achieve high flash point. , good price, low freezing point effect

Inactive Publication Date: 2019-10-11
HEBEI JINGU RECYCLING RESOURCES DEV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The object of the present invention is to provide the process of utilizing biodiesel to produce chlorinated fatty acid methyl esters to solve the problem that the existing biodiesel production process of chlorinated fatty acid methyl esters proposed in the above-mentioned background technology has high cost, low flash point and high freezing point of the finished product , and there is still the problem of physiological toxicity residue in production

Method used

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Embodiment Construction

[0019] The technical solutions in the embodiments of the present invention will be clearly and completely described below. Obviously, the described embodiments are only some of the embodiments of the present invention, but not all of them. Based on the embodiments of the present invention, all other embodiments obtained by persons of ordinary skill in the art without making creative efforts belong to the protection scope of the present invention.

[0020] The invention provides a technical solution:

[0021] Using biodiesel to produce chlorinated fatty acid methyl ester process, biodiesel to produce chlorinated fatty acid methyl ester process synthesis steps are as follows:

[0022] Step 1: Select biodiesel as the main raw material, and the acid value of biodiesel is within 0.2mgKOH / g, and it is anhydrous, impurity-free, colorless and odorless, the reaction raw materials are chlorine, catalyst and ultraviolet light, the protective gas is nitrogen, and the preparation equipment...

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Abstract

The invention discloses a process for producing chloro-fatty acid methyl ester by utilizing biodiesel. The process for producing the chloro-fatty acid methyl ester by utilizing the biodiesel comprisesthe synthetic steps that step 1-6, and in the reaction preparation for the producing the chloro-fatty acid methyl ester by utilizing the biodiesel, the preparation of a preparation reaction is carried out through step 2-5, so that the cost of the preparation through multiple steps is reduced, the cost of capital input is reduced, and preparation equipment is reduced, so that the labor cost is effectively reduced, and the preparation efficiency is effectively improved; in the preparation, protection is carried out through nitrogen, so that a reaction with an air substance is avoided, and the reaction is more efficient and sufficient; the chloro-fatty acid methyl ester prepared through the four steps has good advantages of low cost, high flashing point, low condensation point, no physiological toxicity and the like, has outstanding comprehensive performance, and has more market competition compared with a common plasticizer DOP.

Description

technical field [0001] The invention belongs to the technical field of biodiesel, and in particular relates to a process for producing chlorinated fatty acid methyl esters by using biodiesel. Background technique [0002] Biodiesel refers to vegetable oil (such as rapeseed oil, soybean oil, peanut oil, corn oil, cottonseed oil, etc.), animal oil (such as fish oil, lard, tallow, sheep oil, etc.), waste oil or microbial oil and methanol or ethanol Fatty acid methyl or ethyl esters formed by ester conversion. Biodiesel is a typical "green energy", which has the characteristics of good environmental performance, good engine start performance, good fuel performance, wide source of raw materials, and renewable properties. Vigorously developing biodiesel has important strategic significance for sustainable economic development, promoting energy substitution, reducing environmental pressure, and controlling urban air pollution. [0003] The fuel performance of biodiesel is close t...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07C67/307C07C69/63C07C69/65
CPCC07C67/307C07C69/63C07C69/65Y02E50/10
Inventor 赵敏仲王子腾
Owner HEBEI JINGU RECYCLING RESOURCES DEV
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