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Preparation method of bifunctional hydrogel with adsorption catalysis

An adsorption catalysis, hydrogel technology, applied in chemical instruments and methods, adsorption water/sewage treatment, inorganic chemistry, etc., can solve the problems of complex preparation methods, poor product performance indicators, poor control effects, etc., and achieve high-efficiency degradation ability. , The preparation method is simple, and the dispersibility is improved.

Inactive Publication Date: 2019-10-22
MUDANJIANG NORMAL UNIV
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Problems solved by technology

[0007] In the prior art, the polybutyl acrylate emulsion particles are not introduced into the hydrogel, and the toughness of the hydrogel is not increased
Moreover, the preparation method of the present invention in the prior art is complicated, and the degradation ability to organic dyes in the water body is poor
The control effect of the preparation process parameters in the prior art is poor, resulting in poor product performance indicators and low dye adsorption effect

Method used

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  • Preparation method of bifunctional hydrogel with adsorption catalysis
  • Preparation method of bifunctional hydrogel with adsorption catalysis
  • Preparation method of bifunctional hydrogel with adsorption catalysis

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Embodiment Construction

[0052] In order to make the object, technical solution and advantages of the present invention more clear, the present invention will be further described in detail below in conjunction with the examples. It should be understood that the specific embodiments described here are only used to explain the present invention, not to limit the present invention.

[0053] In the prior art, the polybutyl acrylate emulsion particles are not introduced into the hydrogel, and the toughness of the hydrogel is not increased. Moreover, the preparation method of the present invention in the prior art is complicated, and the degradation ability to organic dyes in water bodies is poor.

[0054] In order to solve the above problems, the present invention will be described in detail below in conjunction with the accompanying drawings.

[0055] Such as figure 1 As shown, the preparation method of the hydrogel with adsorption and catalysis bifunctionality provided by the embodiment of the present...

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Abstract

The invention belongs to the field of environmental protection water treatment, and discloses a preparation method of a bifunctional hydrogel with adsorption catalysis, which prepares polybutyl acrylate emulsion particles. Adding sodium dodecyl sulfate and NaCl into deionized water, and uniformly stirring at normal temperature to obtain transparent micelle aqueous solution; adding a small amount of hydrophobic monomers HM and PBA LPS into the aqueous solution, and uniformly stirring; adding a certain amount of acrylamide, potassium persulfate and Tmeda, and stirring uniformly; Reacting the obtained solution in an oven to obtain hydrogel; Immersed in the prepared aqueous solution of noble metal ions, the hydrogel is separated, reduced by a reducing agent for 1 to 10 hours, and dried to obtain the final product. According to the invention, polybutyl acrylate emulsion particles are introduced into the hydrogel, so that the toughness of the hydrogel is increased. The preparation method issimple and has high-efficiency degradation capability for organic dyes in water.

Description

technical field [0001] The invention belongs to the field of environmental protection water treatment, and in particular relates to a preparation method of hydrogel with adsorption and catalysis dual functions. Background technique [0002] Currently, the closest prior art: [0003] Water pollution is a huge environmental problem, as is the large amount of dye wastewater discharged by the paper, plastic, cosmetic and textile industries, which are non-biodegradable, toxic and carcinogenic. Traditional treatment methods, such as coagulation, solvent extraction and biological treatment, have certain drawbacks. Adsorption is considered to be an inexpensive and technically simple method. Currently, many different kinds of adsorbents have been developed, including activated carbons, resins, and hydrogels. Among them, the hydrogel adsorbent is a novel three-dimensional network structure material with a large number of functional groups, such as hydroxyl and amide groups, and the...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08F265/04C08F220/56C08F220/18C08F226/06B01J20/26B01J20/28C02F1/28B01J20/30
CPCC08F265/04C08F220/18B01J20/267B01J20/264B01J20/28047C02F1/285C08F220/1804C08F220/56
Inventor 崔术新左明辉尹乾柱姜力薛巨坤
Owner MUDANJIANG NORMAL UNIV