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High-tech material for lining of needle-shaped coke rotary kiln and preparation method thereof

A technology of rotary kiln and needle coke, which is applied in the field of high-tech materials for needle coke rotary kiln lining and its preparation, which can solve the problems that restrict the production of needle coke enterprises, and achieve excellent high temperature resistance, good overall structure and long service life Effect

Pending Publication Date: 2019-12-03
巩义市富华耐材有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Two needle coke enterprises in China were forced to reduce production due to the refractory materials used in the rotary kiln after 6 months of operation, which seriously restricted the production of needle coke enterprises

Method used

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  • High-tech material for lining of needle-shaped coke rotary kiln and preparation method thereof
  • High-tech material for lining of needle-shaped coke rotary kiln and preparation method thereof
  • High-tech material for lining of needle-shaped coke rotary kiln and preparation method thereof

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preparation example Construction

[0033] A method for preparing a high-tech material for needle coke rotary kiln lining, comprising the following steps: (1) adding a certain amount of aggregate, fine powder material, and superfine powder to a mixing equipment in sequence according to parts by weight, and mixing uniformly; 2) Add the admixture to the kneading equipment, fully stir and mix evenly to obtain the finished product; (3) testing; (4) packing.

[0034] The detection method is as follows: add the finished product obtained in step (2) into the mold to make a sample block with a length, width and height of 160mm×40mm×40mm, let it stand for 24 hours, demould, and then keep it for three days and then place it in a 110°C refrigerator. Dry in an oven for 24 hours to prepare a sample, and test the compressive strength, bulk density, flexural strength, and linear change rate of the sample.

Embodiment 1

[0036] A high-tech material for needle coke rotary kiln lining, including the following raw materials in parts by weight: 60 parts of aggregate, 25 parts of matrix, 4 parts of superfine powder, and 5 parts of admixture, wherein the aggregate includes electro-fused Mullite particles, the parts by weight of fused mullite particles of each fineness in the aggregate are: 15 parts of fused mullite with a fineness of 5-10mm, 26 parts of fused mullite with a fineness of 3-5mm Stone, 10 parts of 1-3mm fused mullite, 15 parts of 0-1mm fused mullite; the matrix includes 320 mesh and 200 mesh mullite fine powder, and the weight ratio of the two is 1:0.8. The ultrafine powder includes active SiO in a weight ratio of 1:1 2 Superfine powder and α-Al 2 o 3 Ultrafine powder, active SiO 2 SiO in superfine powder 2 The content is 90.9% and active SiO 2 The fineness of ultrafine powder is less than 10μm; α-Al 2 o 3 Al in ultrafine powder 2 0 3 The content of 99.43% and α-Al 2 o 3 The ...

Embodiment 2

[0039] A high-tech material for the lining of a needle coke rotary kiln, comprising the following raw materials in parts by weight: 75 parts of aggregate, 15 parts of matrix, 10 parts of superfine powder, and 1 part of admixture, wherein the aggregate includes electric melting Mullite particles, the parts by weight of the fused mullite particles of each fineness in the aggregate are: 25 parts of fused mullite with a fineness of 5-10mm, and 18 parts of fused mullite with a fineness of 3-5mm Stone, 19 parts of 1-3mm fused mullite, 10 parts of 0-1mm fused mullite; the matrix includes 320 mesh and 200 mesh mullite fine powder, the ratio of the two is 1:2. The ultrafine powder includes active SiO in a weight ratio of 1:1 2 Superfine powder and α-Al 2 o 3 Ultrafine powder, active SiO 2 SiO in superfine powder 2 The content is 90.9% and active SiO 2 The fineness of ultrafine powder is less than 10μm; α-Al 2 o 3 Al in ultrafine powder 2 0 3 The content of 99.43% and α-Al 2 o...

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Abstract

The invention relates to the technical field of needle-shaped coke rotary kilns, and specifically provides a high-tech material for a lining of a needle-shaped coke rotary kiln. The material comprisesan aggregate, a matrix, an ultrafine powder, and an admixture, and weight parts of each component are as follows: 60-75 parts of the aggregate, 15-25 parts of the matrix, 4-10 parts of the ultrafinepowder, and 1-5 parts of the admixture. A preparation method of the material comprises the following steps: (1) successively adding a certain amount of the aggregate, a fine powder material, and the ultrafine powder into mixing equipment according to the weight parts, and performing uniform mixing; (2) adding the admixture into the mixing equipment, and performing thorough stirring and uniform mixing to obtain a finished product; (3) performing detection; and (4) performing packaging. The high-tech material for the lining of the needle-shaped coke rotary kiln produced by the method shows excellent properties such as high-temperature resistance, wear resistance, scouring resistance, erosion resistance, and thermal shock resistance, an overall structure is good, and the service life is long,so that the material is an ideal material suitable for a lining of a needle-shaped coke rotary kiln under a temperature of 1450 DEG C-1550 DEG C for a long time.

Description

technical field [0001] The invention relates to the technical field of a needle coke rotary kiln, in particular to a high-tech material for the lining of a needle coke rotary kiln and a preparation method thereof. Background technique [0002] Needle coke is the raw material for preparing high-temperature carbon products such as ultra-high-power electrodes, special carbon materials, and carbon fibers. Calcination is an important process in the production of needle coke, which directly affects the quality of electrode products. At present, domestic needle coke calcination equipment is generally suitable for calcination of petroleum coke. The common ones are rotary kiln, tank furnace, and rotary bed. In comparison, the rotary kiln has simple structure, low construction cost, large output, The advantages of simple operation and high level of automatic control are usually used as the calcination production equipment of needle coke. When the rotary kiln calcines needle coke, the...

Claims

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Application Information

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IPC IPC(8): C04B35/66C04B35/185
CPCC04B35/66C04B35/185C04B2235/3418C04B2235/3217C04B2235/444C04B2235/447C04B2235/77C04B2235/96C04B2235/9615
Inventor 刘龙邓海亮邓海峰
Owner 巩义市富华耐材有限公司