Composite material for adsorbing formaldehyde, and preparation method thereof
A technology for adsorbing formaldehyde and composite materials, applied in the field of composite materials for adsorbing formaldehyde and its preparation, can solve the problem of low formaldehyde removal rate and achieve the effect of enriching the porous structure
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Embodiment 1
[0040] The preparation method of the composite material for removing formaldehyde of the present embodiment comprises the following steps:
[0041] 1) Add 0.5g of polyvinyl alcohol into 75mL of water, slowly raise the temperature to 65°C and stir continuously to dissolve it completely, and obtain an aqueous solution of polyvinyl alcohol, which is then added to the flask for later use;
[0042] Mix 1.8g of N,N'-methylenebisacrylamide, 4.5g of methyl methacrylate, and 10g of liquid paraffin, stir for 10min, add 0.1g of initiator azobisisobutyronitrile to the mixture and mix , to get a mixture;
[0043] 2) Slowly add the above mixed solution to the aqueous solution of polyvinyl alcohol in the flask under stirring condition. After the addition, put the flask in a water bath at 60°C, and continue to stir and react at a speed of 250rpm for 12h; after the reaction, the solid-liquid Separation: Mix the solid with 100 mL of absolute ethanol and stir for 15 minutes, separate the solid ...
Embodiment 2
[0048] The preparation method of the composite material for removing formaldehyde of the present embodiment comprises the following steps:
[0049] 1) Add 0.8g of polyvinyl alcohol into 80mL of water, slowly raise the temperature to 70°C and stir continuously to dissolve it completely, and obtain an aqueous solution of polyvinyl alcohol, which is then added to the flask for later use;
[0050] Mix 2g of N,N'-methylenebisacrylamide, 6g of methyl methacrylate, and 15g of liquid paraffin, stir for 15min, add 0.2g of initiator azobisisobutyronitrile into the mixture and mix to obtain mixed solution;
[0051] 2) Slowly add the above mixed solution into the polyvinyl alcohol aqueous solution in the flask under stirring condition. After the addition, put the flask in a water bath at 60°C, and continue to stir and react at a speed of 200rpm for 10h; after the reaction, the solid-liquid Separation: Mix the solid with 100 mL of absolute ethanol and stir for 20 minutes, separate the sol...
Embodiment 3
[0056] The preparation method of the composite material for removing formaldehyde of the present embodiment comprises the following steps:
[0057] 1) Add 1.5g of polyvinyl alcohol into 100mL of water, slowly raise the temperature to 75°C and stir continuously to dissolve it completely, and obtain an aqueous solution of polyvinyl alcohol, which is then added to the flask for later use;
[0058] Mix 2.5g of N,N'-methylenebisacrylamide, 10g of methyl methacrylate, and 18g of liquid paraffin, stir for 20min, add 0.5g of initiator azobisisobutyronitrile to the mixture, get the mixture;
[0059] 2) Slowly add the above mixed solution to the aqueous solution of polyvinyl alcohol in the flask under stirring conditions. After the addition, put the flask in a water bath at 60°C, and continue to stir and react at a speed of 200rpm for 15h; after the reaction, the solid-liquid Separation: Mix the solid with 150 mL of absolute ethanol and stir for 20 minutes, separate the solid from the ...
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Abstract
Description
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