Unlock instant, AI-driven research and patent intelligence for your innovation.

A polymer oil-absorbing material and its preparation method

A technology of oil-absorbing materials and polymers, which is applied in the field of polymer oil-absorbing materials and their preparation, can solve the problems of complex preparation process, unfavorable product promotion and application of industrial scale-up products, and high cost, and achieve simple process and low requirements for equipment and reaction conditions , the effect of large oil absorption

Active Publication Date: 2021-12-03
HUNAN QIWEI TECH CO LTD
View PDF7 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

These methods require specific means to remove the porogen added in the preparation process, the preparation process is complicated, the cost is high, and it is not conducive to the industrial amplification of the product and the popularization and application of the product.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] Preparation method of polymer oil absorbing material, including steps:

[0028]Step S1, poly 1-p-Toluenesulfonyl-2,5-pyrrolidine dimethal 2,3-difluorofunamate: 1-p-toluenesulfonyl-2,5-pyrrolidine dimethalol 18.8g , 2,3-difluorofumin acid 10g, tetrabutyl titanate, tetrachloride 1 g added to dimethyl sulfoxide 90g, stirred for 20 minutes, resulting in a reaction solution, then transfer the reaction solution to a high pressure reaction In the kettle, the air was placed in nitrogen, and then the esterification reaction was carried out at a temperature of 230 ° C, the pressure pressure was 30 kPa, and the esterification was completed, and the pressure was completed to normal pressure; then in vacuum conditions, the temperature was controlled at 240. When the reaction was stirred at ° C, the reaction was stirred at the end of the reaction, and the liquid was taken out and the mass fraction was 0.5% aqueous sodium hydroxide solution, and then the sinking of the sketch was washed 3...

Embodiment 2

[0034] Preparation method of polymer oil absorbing material, including steps:

[0035] Step S1, poly 1-p-Toluenesulfonyl-2,5-pyrrolidine dimethal 2,3-difluorofunamate: 1-p-toluenesulfonyl-2,5-pyrrolidine dimethalol 18.8g , 2,3-difluorofumin acid 10 g, titanium dioxide 4.5 g, L, 4-naphthoquinone 1 g addition to N, N-dimethylformamide 110g, stirred for 23 minutes, resulting in the reaction solution, then the reaction solution Transfer to the high pressure reactor, the air is placed in the air, and then the esterification reaction is performed at a temperature of 250 ° C, the pressure pressure is 50 kPa, and the esterification is ended, and the pressure is completed to the normal pressure; then under vacuum conditions. However, the control temperature is between 250 ° C, stirred at a stirred reaction, and then cool to room temperature after the reaction, exit and deposit in aqueous sodium hydroxide solution in a mass fraction, then washed with ethanol 4 times, then Ethanol was evapor...

Embodiment 3

[0041] Preparation method of polymer oil absorbing material, including steps:

[0042] Step S1, poly 1-p-Toluenesulfonyl-2,5-pyrrolidine dimethal 2,3-difluorofunamate: 1-p-toluenesulfonyl-2,5-pyrrolidine dimethalol 18.8g 10 g of 2,3-difluoromaic acid, 5 g of titanium tide, tetrachloroquinone 1 g is added to N, N-dimethylacetamide 125g, stirred for 25 minutes, resulting in reaction solution, then transfer the reaction solution In the high pressure reactor, the air is placed in the air, then the esterification reaction is carried out at a temperature of 260 ° C, the pressure pressure 70 kPa, and the esterification, pressure is completed to normal pressure; then in vacuum conditions, The control temperature is between 255 ° C, stirred for 15h, and then cool to room temperature after the reaction is completed, exit and sink in aqueous sodium hydroxide solution in a mass fraction, and then washed with ethanol 5 times, and then Ethanol is evaporated to give poly 1-p-p-toluenesulfonyl-2,...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
viscosityaaaaaaaaaa
Login to View More

Abstract

The invention discloses a preparation method of a polymer oil-absorbing material, which is characterized in that it comprises the following steps: step S1, poly 1-p-toluenesulfonyl-2,5-pyrrolidinedimethanol 2,3-difluorofumaric acid Preparation of ester, step S2, modification of poly 1-p-toluenesulfonyl-2,5-pyrrolidinedimethanol 2,3-difluorofumarate, step S3, preparation of copolymer, step S4, porogenic . The invention also discloses the polymer oil-absorbing material prepared according to the preparation method of the polymer oil-absorbing material. The polymer oil-absorbing material disclosed by the invention has better mechanical properties, larger oil absorption capacity, better oil absorption effect, faster oil absorption speed, better comprehensive performance, and higher economic value, social value and ecological value.

Description

Technical field [0001] The present invention relates to the field of oil absorbing materials, and more particularly to a polymer oil absorbing material and a preparation method thereof. Background technique [0002] In recent years, with the development of the world industry, as the exploitation, production, transportation and use of various oils of industrial blood, oil is transported, replaced, and used during transportation, due to hourglass, leakage, sputtering, etc. Will affect the workplace and the ecological environment around the contamination; the production process of oil and industries, refining and petrochemical, food industry, etc. also produce a large amount of oil-containing wastewater, pollution water environment, harm aquatic Biology, even through the food chain into the human body, harm human health; there will be a large amount of oil gas pollution atmosphere in the catering industry and daily life; wash the kitchen utensils in daily life, the large amount of w...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): B01D17/022
CPCB01D17/0202
Inventor 程旺生钟自强
Owner HUNAN QIWEI TECH CO LTD
Features
  • R&D
  • Intellectual Property
  • Life Sciences
  • Materials
  • Tech Scout
Why Patsnap Eureka
  • Unparalleled Data Quality
  • Higher Quality Content
  • 60% Fewer Hallucinations
Social media
Patsnap Eureka Blog
Learn More

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.

© 2025 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com