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Method for preparing carbon nanotube reinforced aluminum-based composite material

A technology of carbon nanotubes and composite materials, applied in metal material coating technology, ion implantation plating, coating, etc., can solve the problems of high cost of composite materials, unsuitable for popularization and application, etc., and achieve the improvement of mechanical properties and preparation methods Simple and easy to use, the effect of enhancing the binding force

Inactive Publication Date: 2019-12-31
淮安正天新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the cost of composite materials prepared by this method is high, and it is not suitable for popular application.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] A method for preparing carbon nanotube-reinforced aluminum matrix composites, comprising the steps of:

[0022] Step 1, the following raw materials are weighed in parts by weight: 18 parts of nano-aluminum, 1 part of nano-titanium dioxide, 20 parts of carbon nanotubes, 1 part of bamboo fiber, 24 parts of polyethylene glycol, 45 parts of aluminum oxide, polyethylene glycol 40 parts, 1 part of modified starch; the modified starch is formed by mixing starch, chitosan and copper sulfate according to a molar ratio of 3:1:2; the diameter of carbon nanotubes is 10 nm, and the length is 20 μm;

[0023] Step 2. After immersing the carbon nanotubes in the modified starch and freeze-drying at low temperature, put them into a ball mill and grind them. The ball milling speed is 100rpm, and the material of the balls is 3mm quartz sand. Through the magnetic sputtering technology, the carbon nanotubes are sputtered on the surface of the carbon nanotubes in turn. Inject nano-titanium di...

Embodiment 2

[0027] A method for preparing carbon nanotube-reinforced aluminum matrix composites, comprising the steps of:

[0028] Step 1, weigh the following raw materials in parts by weight: 20 parts of nano-aluminum, 2 parts of nano-titanium dioxide, 24 parts of carbon nanotubes, 3 parts of bamboo fiber, 35 parts of polyethylene glycol, 48 parts of aluminum oxide, polyethylene glycol 48 parts, 2 parts of modified starch; the modified starch is mixed by starch, chitosan and copper sulfate according to the molar ratio of 5:1:2; the diameter of the carbon nanotube is 14nm, and the length is 22μm

[0029] Step 2. After immersing the carbon nanotubes in the modified starch and freeze-drying at low temperature, put them into a ball mill and grind them. The ball milling speed is 110rpm, and the material of the balls is 4mm quartz sand. Through the magnetic sputtering technology, the carbon nanotubes are sputtered on the surface of the carbon nanotubes in turn. Spray nano-titanium dioxide, nan...

Embodiment 3

[0033] A method for preparing carbon nanotube-reinforced aluminum matrix composites, comprising the steps of:

[0034] Step 1, the following raw materials are weighed in parts by weight: 28 parts of nano-aluminum, 4 parts of nano-titanium dioxide, 28 parts of carbon nanotubes, 8 parts of bamboo fiber, 43 parts of polyethylene glycol, 60 parts of aluminum oxide, polyethylene glycol 50 parts, 3 parts of modified starch; modified starch is composed of starch, chitosan and copper sulfate according to the molar ratio of 6:1:4; the diameter of carbon nanotubes is 20nm, and the length is 30μm

[0035] Step 2. After immersing the carbon nanotubes in the modified starch and freeze-drying at low temperature, put them into a ball mill and grind them. The ball milling speed is 120rpm, and the material of the balls is 5mm quartz sand. Through the magnetic sputtering technology, the carbon nanotubes are sputtered on the surface of the carbon nanotubes in turn. Spray nano-titanium dioxide an...

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Abstract

The invention discloses a method for preparing a carbon nanotube reinforced aluminum-based composite material. The method comprises the following steps: weighing the following raw materials, by weight, 18-28 parts of nano-aluminum, 1-4 parts of nanometer titanium dioxide, 20-28 parts of carbon nanotubes, 1-8 parts of bamboo fibers, 24-43 parts of polyvinyl diol, 45-60 parts of aluminum oxide, 40-50 parts of polyethylene glycol and 1-3 parts of modified starch; immersing the carbon nanotubes in the modified starch, carrying out low-temperature freeze drying, adding the obtained material into aball mill, grinding the material, and sputtering the ground material by using a magnetic sputtering technology to obtain modified carbon nanotubes; mixing the aluminum oxide with the bamboo fibers, adding the obtained mixture into the ball mill, ball-milling the mixture, then adding the polyvinyl glycol and polyethylene glycol, performing uniform stirring, adding the modified carbon nanotubes, continuously performing stirring, adding the obtained mixture into a double-screw extruder, and pressing the mixture to obtain the aluminum-based composite material. The composite material prepared in the invention has the characteristics of light weight and excellent mechanical properties, and the preparation method is simple, is easy to implement, and is suitable for industrial production.

Description

technical field [0001] The invention relates to the field of composite materials, in particular to a method for preparing carbon nanotube-reinforced aluminum-based composite materials. Background technique [0002] Composite materials refer to materials formed by combining two or more phases of materials together. Most of the composite materials widely used in modern times are composed of various high-performance fibers as the reinforcing phase and resin as the matrix phase. Aluminum matrix composites have high specific strength, specific modulus, good electrical and thermal conductivity, and high temperature performance. They have been applied in aerospace, automotive, and microelectronics fields and have attracted more and more attention. Carbon nanotubes have a unique structure and excellent physical and chemical properties (the Young's modulus can reach 1-1.8TPa, the tensile strength can reach 150GPa, and the density can reach 1.2-1.8g / cm 3 , the thermal expansion coef...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L71/02C08L97/02C08L3/02C08L5/08C08K13/06C08K9/10C08K3/04C08K3/22C08K3/08C22C1/04C22C1/05C22C21/00C23C14/35
CPCC08K2003/0812C08K2003/2227C08K2201/011C08L71/02C08L2205/025C08L2205/035C08L2205/16C22C1/0416C22C1/05C22C21/00C23C14/35C08L97/02C08L3/02C08L5/08C08K13/06C08K9/10C08K3/041C08K3/22C08K3/08
Inventor 李铜玲
Owner 淮安正天新材料科技有限公司
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