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Preparation method of compound plant extract capable of promoting salivation and increasing moisture and cold extraction electronic cigarette oil

A plant extract and compound technology, applied in the field of cold-extracted e-liquid, can solve the problems of throat irritation, dry throat, burnt feeling, etc., to enhance the moist feeling of the throat, reduce throat irritation, increase The effect of taste characteristics

Inactive Publication Date: 2019-12-31
SHENZHEN BOTON FLAVORS & FRAGRANCES
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Therefore, at present, various natural plants are extracted to obtain extracts with certain active ingredients as the base oil of e-cigarette oil combined with other flavors to form e-cigarette oil, or extracted as e-cigarette oil alone, which contains natural flavors advantages, but now there are not many developments for this kind of natural plants, and there are few types, mainly tea ingredients and fruit flavors are the mainstream; secondly, the current methods for extracting natural plants generally use simple distillation, centrifugation, Conventional methods such as filtration extraction to prepare plant extracts make it easy for macromolecules and polar compounds in natural plants to be extracted and mixed in the extract. It is difficult to be atomized, and it is easy to cause some adverse effects such as burnt feeling and blockage of the atomizer when inhaling. It is very irritating to the throat, resulting in dry throat and poor comfort, which brings discomfort to users. For an ideal experience, further refined plant extracts and a combination of plant extracts are needed to improve throat irritation and enhance throat hydration

Method used

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  • Preparation method of compound plant extract capable of promoting salivation and increasing moisture and cold extraction electronic cigarette oil
  • Preparation method of compound plant extract capable of promoting salivation and increasing moisture and cold extraction electronic cigarette oil

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] Accurately weigh 40g of fresh roses, 220g of honeysuckle, 80g of aloe vera, 250g of green olives, 200g of green plums, and 60g of green tea, and place them on a vacuum freeze dryer at a pre-freezing rate of 0.7℃ / min, drying chamber pressure 84Pa, heating plate Freeze-dried at a temperature of 40℃ for 26 hours, then quickly pulverize, pass through a 120-mesh screen, and load the lyophilized raw material powder into a 2cm*100cm glass chromatography column and connect the glass chromatography column Add 250ml of propylene glycol into the upper liquid storage bottle, open the valve, control the flow rate at 1ml / min, and collect 120ml of extract; the extract is subjected to high-speed refrigerated centrifugation at a temperature of 4℃ and a rotational speed of 8000r / min. Compound plant extract 1; take 2.0 parts of compound plant extract 1, 2.0 parts of leaf alcohol, 1.5 parts of melon aldehyde, 3.5 parts of phenethyl alcohol, 6.0 parts of linalool, 2.0 parts of leaf alcohol ac...

Embodiment 2

[0031] Accurately weigh 35g of fresh roses, 180g of honeysuckle, 60g of aloe vera, 230g of green olives, 180g of green plums, and 40g of green tea, and place them on a vacuum freeze dryer at a pre-freezing rate of 0.6°C / min, drying chamber pressure 88Pa, heating plate After being freeze-dried for 30 hours at a temperature of 38℃, the powder is quickly pulverized, and the lyophilized raw material powder is loaded into a 2.5cm*80cm glass chromatography column through a 120-mesh screen and connected to the glass chromatography Add 250ml of propylene glycol into the reservoir on the top of the column, open the valve, control the flow rate at 1.5ml / min, and collect 100ml of extract; freeze the extract at a high speed at a temperature of 4℃ and a rotation speed of 5000r / min Centrifuge to obtain compound plant extract 2; take 4.0 parts of compound plant extract 2, 3.0 parts of leaf alcohol, 2.0 parts of melon aldehyde, 3.0 parts of phenethyl alcohol, 5.0 parts of linalool, 2.5 parts of...

Embodiment 3

[0033] Accurately weigh 48g of fresh roses, 160g of honeysuckle, 50g of aloe vera, 230g of green olives, 160g of green plum, and 35g of green tea. Place them on a vacuum freeze dryer at a pre-freezing rate of 0.8℃ / min, drying chamber pressure 75Pa, heating plate After 42 hours of freeze-drying at a temperature of 45°C, it is quickly pulverized, and the lyophilized raw material powder is loaded into a 2.5cm*80cm glass chromatography column through a 200-mesh screen, and connected to the glass chromatography Add 220ml of propylene glycol to the reservoir on the top of the column, open the valve, control the flow rate at 2.0ml / min, collect 150ml of extract, and perform high-speed refrigerated centrifugation at a temperature of 25°C and a rotation speed of 10000r / min. Compound plant extract 3; take 6.0 parts of compound plant extract 3, 2.8 parts of leaf alcohol, 2.2 parts of melon aldehyde, 3.5 parts of phenethyl alcohol, 6.8 parts of linalool, 2.4 parts of leaf alcohol acetate, 0....

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Abstract

The invention discloses a preparation method of a compound plant extract capable of promoting salivation and increasing moisture, and cold extraction electronic cigarette oil. The method comprises thefollowing steps: fresh plant materials such as fresh rose flowers, honeysuckle flowers, aloe vera, green olives, green plums and green tea are selected to form a compound plant combination, the compound plant combination are subjected to vacuum freeze drying treatment, and crushing is performed to obtain freeze-dried raw material powder; and cold extraction is performed on the freeze-dried raw material powder by using a chromatographic column to obtain the compound plant extract. The method can keep the fragrance of the fresh plant materials, retain most of other functional active substanceswith lower boiling points and heat sensitivity, and reduce dissolution of macromolecular substances; the compound plant extract can remarkably reduce throat irritation and enhance throat moisturizingfeeling; and the obtained compound plant extract is combined with an electronic cigarette essence base to be applied to the electronic cigarette oil, the taste characteristic of the electronic cigarette oil is improved, some adverse effects such as scorching feeling and atomizer blockage easily caused by natural extract atomization in the smoking process are reduced, and the user experience is improved.

Description

Technical field [0001] The present invention relates to the technical field of electronic cigarette oil, in particular to a method for preparing a body fluid-enhancing compound plant extract, a body fluid-enhancing compound plant extract and cold-extracted electronic cigarette oil. Background technique [0002] E-cigarettes are electronic products that imitate cigarettes and have the same appearance, smoke, taste and feel as cigarettes. The core part of e-cigarettes is e-liquid. Existing e-liquids are mainly prepared from chemical monomer raw materials. These e-liquids still have many defects when inhaling, such as great irritation to the throat. Causes dry throat, poor comfort, and undesirable experience for users; [0003] Plant extracts are based on plants as raw materials. According to the needs of the use of the final product extracted, through the physical and chemical extraction and separation process, one or more effective ingredients in the plant are obtained and enriched...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/02C11B9/00A24B15/16A24F47/00
CPCC11B9/025C11B9/0003A24B15/16A24B15/167
Inventor 强耀锋卢丽娟王晶李剑政管舒婷
Owner SHENZHEN BOTON FLAVORS & FRAGRANCES
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