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Production method of high-sulfur full-water-soluble nitrosulfur-based nitrogen fertilizer particles

A production method, fully water-soluble technology, applied in nitrogen fertilizer, ammonium nitrate fertilizer, fertilization device, etc., can solve problems such as inability to form eutectic, thick slurry, and inability to continue normal production

Active Publication Date: 2020-01-10
SHANXI HUAXIN COKE & COAL IND GRP CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

During the mixing process, the ammonium sulfate solid is only suspended in the ammonium nitrate melt, and cannot be organically combined to form a eutectic, resulting in a thick slurry during the production process, and the produced granular product has many heterogeneous particles, low strength, and is easy to Agglomeration and pulverization, unable to continue normal production, has become a difficult problem in the industry

Method used

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  • Production method of high-sulfur full-water-soluble nitrosulfur-based nitrogen fertilizer particles
  • Production method of high-sulfur full-water-soluble nitrosulfur-based nitrogen fertilizer particles
  • Production method of high-sulfur full-water-soluble nitrosulfur-based nitrogen fertilizer particles

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Effect test

Embodiment 1

[0044] A method for producing quick-acting and long-acting high-sulfur full water-soluble nitrosulfur-based fertilizer granules, comprising the following steps:

[0045] 1) 95% of the ammonium nitrate produced by the ammonium nitrate plant is transported to the second-stage evaporation of ammonium nitrate in the high tower through a melt pump, and concentrated into a 99% ammonium nitrate solution, which accounts for 44% of the total mass ratio of ammonium nitrate after being measured by a mass flow meter The solution enters the primary mixing tank; at the same time, in the primary mixing tank, add a thickening agent (sodium dodecylsulfonate) accounting for 1% of the total mass ratio and a conditioning agent accounting for 3% of the total mass ratio after being metered by the metering belt under the tower (polyvinyl acetate) and solid ammonium sulfate accounting for 35% of the total mass ratio are fully mixed under stirring, and the temperature is controlled to 165-170°C.

[00...

Embodiment 2

[0049] A method for producing quick-acting and long-acting high-sulfur full water-soluble nitrosulfur-based fertilizer granules, comprising the following steps:

[0050] 1) 95% of the ammonium nitrate produced by the ammonium nitrate plant is transported to the second-stage evaporation of ammonium nitrate in the high tower through a melt pump, and concentrated into a 99% ammonium nitrate solution, which accounts for 51% of the total mass ratio of ammonium nitrate after being measured by a mass flow meter The solution enters the first-level mixing tank; at the same time, add a thickening agent (sodium dodecylsulfonate) accounting for 1% of the total mass ratio and a conditioning agent accounting for 3% of the total mass ratio after being metered by the metering belt under the tower in the primary mixing tank (polyvinyl acetate) and solid ammonium sulfate accounting for 25% of the total mass ratio are fully mixed under stirring, and the temperature is controlled to 165-170°C.

...

Embodiment 3

[0054] A method for producing quick-acting and long-acting high-sulfur full water-soluble nitrosulfur-based fertilizer granules, comprising the following steps:

[0055] 1) 95% of the ammonium nitrate produced by the ammonium nitrate plant is transported to the second-stage evaporation of ammonium nitrate in the high tower through a melt pump, and concentrated into a 99% ammonium nitrate solution, which accounts for 58% of the total mass ratio of ammonium nitrate after being measured by a mass flow meter Solution enters in the first-level mixing tank; Add simultaneously in the first-level mixing tank and account for 1% thickening agent (sodium lauryl sulphate) of the total mass ratio and the conditioner ( polyacrylamide) and solid ammonium sulfate accounting for 25% of the total mass ratio are fully mixed under stirring, and the temperature is controlled to 165-170°C.

[0056] 2) 13% of the total mass ratio of solid ammonium sulfate enters the secondary mixing tank together wi...

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Abstract

The invention discloses a production method of high-sulfur full-water-soluble nitrosulfur-based nitrogen fertilizer particles. The production method comprises the following steps: 1) concentrating ammonium nitrate into a 99% ammonium nitrate solution, and adding 44-58% by mass of the ammonium nitrate solution into a primary mixing tank; 2) adding 1-2% by mass of a thickness reducer, 2-4% by mass of a conditioner and 25-35% by mass of solid ammonium sulfate into the primary mixing tank, and performing full mixing while stirring; (3) allowing 13-20% by mass of solid ammonium sulfate, a return material obtained after finished product screening and a mixed slurry overflowing out of the primary mixing tank to enter a secondary mixing tank, and performing uniform mixing while strong stirring; and 4) continuously and strongly stirring the obtained slurry in a ternary mixing tank, carrying out shearing emulsification and sufficient grinding on the obtained slurry overflowing the mixing tank, allowing the ground slurry to overflow into a mechanical granulator, spraying the slurry by the granulator, and carrying out tower bottom roller air cooling, screening, secondary powder flow cooler cooling and DMPP spraying in a coating machine to obtain the non-caking, quick-acting, long-acting and full-water-soluble high-sulfur and high-ammonium nitrogen nitrosulfur-based nitrogen fertilizer.

Description

technical field [0001] The invention belongs to the technical field of chemical fertilizer production, and in particular relates to a production method of high-sulfur fully water-soluble nitro-nitrogen fertilizer granules. Background technique [0002] At present, domestic nitro fertilizers have high nitrate nitrogen content and low ammonium nitrogen content to meet the needs of plant growth, which will cause excessive nitrate nitrogen to cause nitrogen leaching loss, not only causing a large waste of nitrogen fertilizer, but also increasing Agricultural investment costs, but also lead to serious pollution of surface water and groundwater, resulting in eutrophication of water bodies, which seriously damages the ecological balance; while the low ammonium nitrogen leads to insufficient "stamina" of fertilizer efficiency during use, and there is a phenomenon of defertilization. Secondary topdressing is often required, which is especially obvious in field crops, so it is urgent ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C05G3/00
CPCC05C1/00C05G3/00
Inventor 李腾飞张梓榆崔瑞波吕聪
Owner SHANXI HUAXIN COKE & COAL IND GRP CO LTD
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