Graphene oxide-nano mineral enhanced geopolymer material and preparation method thereof
A technology of geopolymer and graphene, which is applied in the field of graphene oxide-nano-mineral reinforced geopolymer materials and its preparation, can solve the problems of uniform dispersion restricting large-scale applications, and the enhanced performance has not been fully exerted, achieving excellent Effects of compactness and mechanical strength, reduction of total porosity, improvement of quantity and uniformity
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Embodiment 1
[0020] 1) Preparation of geopolymer reaction powder: 240g of metakaolin, 150g of fly ash, 30g of granulated blast furnace slag, 18g of Portland cement, and 12g of nano-silicon dioxide were mixed, stirred and ground in proportion;
[0021] 2) Preparation of graphene oxide-sodium hydroxide solution: 18 g of solid sodium hydroxide, 39 g of deionized water, and 3 g of graphene oxide were mixed, and obtained by ultrasonic dispersion at 50 Hz for 60 minutes;
[0022] 3) Prepare graphene oxide-alkali excitation solution: mix 120g liquid sodium silicate with the graphene oxide-sodium hydroxide solution obtained in step 2), and 50 Hz ultrasonic dispersion for 60 minutes to form a uniform graphene oxide-alkali excitation solution;
[0023] 4) Preparation of graphene oxide-nanometer mineral-enhanced geopolymer material: continuously stir the graphene oxide-alkali excitation solution obtained in step 3), and add the geopolymer reaction powder obtained in step 1), and mix evenly to obtain ...
Embodiment 2
[0025] 1) Preparation of geopolymer reaction powder: 246g of metakaolin, 153g of fly ash, 45g of granulated blast furnace slag, 24g of Portland cement, and 12g of nano-silicon dioxide were mixed, stirred and ground in proportion;
[0026] 2) Preparation of graphene oxide-sodium hydroxide solution: 21 g of solid sodium hydroxide, 42 g of deionized water, and 6 g of graphene oxide were mixed, and obtained by ultrasonic dispersion at 50 Hz for 80 minutes;
[0027] 3) Prepare graphene oxide-alkali excitation solution: mix 135g liquid sodium silicate with the graphene oxide-sodium hydroxide solution obtained in step 2), and 50 Hz ultrasonic dispersion for 60 minutes to form a uniform graphene oxide-alkali excitation solution;
[0028] 4) Preparation of graphene oxide-nanometer mineral-enhanced geopolymer material: continuously stir the graphene oxide-alkali excitation solution obtained in step 3), and add the geopolymer reaction powder obtained in step 1), and mix evenly to obtain ...
Embodiment 3
[0030] 1) Preparation of geopolymer reaction powder: 210g of metakaolin, 135g of fly ash, 30g of granulated blast furnace slag, 15g of Portland cement, and 6g of nano-silicon dioxide were mixed, stirred and ground in proportion;
[0031] 2) Preparation of graphene oxide-sodium hydroxide solution: 15 g of solid sodium hydroxide, 30 g of deionized water, and 3 g of graphene oxide were mixed, and obtained by ultrasonic dispersion at 40 Hz for 60 minutes;
[0032] 3) Preparation of graphene oxide-alkali excitation solution: 105g of liquid sodium silicate was mixed with the graphene oxide-sodium hydroxide solution obtained in step 2), and 40 Hz ultrasonic dispersion was performed for 30 minutes to form a uniform graphene oxide-alkali excitation solution;
[0033] 4) Preparation of graphene oxide-nanometer mineral-enhanced geopolymer material: continuously stir the graphene oxide-alkali excitation solution obtained in step 3), and add the geopolymer reaction powder obtained in step 1...
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