Quick-positioning two-component acrylate structural adhesive and preparation method and use method thereof

A technology of structural adhesives and acrylates, applied in the directions of adhesives, adhesive additives, non-polymer adhesive additives, etc., can solve the problems of shortening the room temperature operation time and increasing the difficulty of operation, and achieves a large adjustable range and comprehensive Excellent performance, fast positioning effect

Inactive Publication Date: 2020-04-28
YANTAI SEAYU NEW MATERIALS CORP LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Conventional methods to speed up positioning usually use highly active monomers or resins with active groups, but when such methods in

Method used

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  • Quick-positioning two-component acrylate structural adhesive and preparation method and use method thereof
  • Quick-positioning two-component acrylate structural adhesive and preparation method and use method thereof
  • Quick-positioning two-component acrylate structural adhesive and preparation method and use method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] A component

[0032]

[0033]

[0034] B component

[0035] component name Component amount Diethylene glycol dibenzoate 30 Benzoyl peroxide 32 Bisphenol A epoxy resin 30 Modified amine latent curing agent 5 pigment 3

[0036] Preparation Process:

[0037] Preparation of component A: Accurately weigh methyl methacrylate, hydroxyethyl methacrylate, tetrahydrofuran acrylate, methacrylic acid, hydroquinone, EDTA-Na, mix well; then add ABS resin, hydrogenated nitrile rubber , stir to dissolve completely; add polyurethane modified acrylic resin, N,N-dimethyl-p-toluidine, zinc diethyldithiocarbamate, PM-2, mercaptan curing agent, stir evenly, and finally add gas phase Stir the white carbon black evenly, hold the vacuum for degassing, and discharge the material to obtain component A.

[0038] Preparation of component B: Accurately weigh diethylene glycol dibenzoate, benzoyl peroxide, and bisphenol A epoxy resin, stir well t...

Embodiment 2

[0041] A component

[0042]

[0043]

[0044] B component

[0045] component name Component amount Dioctyl adipate 30 Benzoyl peroxide 32 Bisphenol F epoxy resin 30 Modified amine latent curing agent 5 pigment 3

[0046] Preparation Process:

[0047] Preparation of component A: Accurately weigh methyl methacrylate, hydroxypropyl methacrylate, tetrahydrofuran acrylate, methacrylic acid, 2-tert-butylhydroquinone, EDTA-Na and mix evenly; then add MBS resin, Polyacrylate rubber, stir to dissolve completely; add epoxy-modified acrylic resin, N,N-dihydroxyethyl-p-toluidine, triphenylphosphine, PM-2010SP, mercaptan, stir evenly, and finally add fume white Stir the carbon black evenly, hold the vacuum for degassing, and discharge to obtain component A.

[0048] Preparation of component B: Accurately weigh dioctyl adipate, benzoyl peroxide, and bisphenol F epoxy resin, stir thoroughly to dissolve them completely, add modified amine ...

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Abstract

The invention discloses a quick-positioning two-component acrylate structural adhesive and a preparation method and a use method thereof. The adhesive comprises a component A and a component B, an acrylate structural adhesive and an epoxy structural adhesive are organically combined together by adopting a blending mode, and thiol curing agents, epoxy resin and epoxy latent curing agents are addedinto different components, so that the thiol curing agents, the epoxy resin and the epoxy latent curing agents are mutually promoted to react. When the component A and the component B are used after being mixed according to the volume ratio of 10:1, the storage is stable at normal temperature, and the operation time is longer; the thiol curing agent of the component A and the epoxy resin of the component B can be initiated to react by low-temperature heating to achieve the quick-positioning effect, and the generated heat is used for initiate the acrylic acid system reaction to form an interpenetration network structure, and the acrylate structural adhesive and the epoxy structural adhesive are organically combined, the adjustable range of raw materials is large, and the structural adhesivewith excellent comprehensive performance is obtained through blending modification.

Description

technical field [0001] The invention belongs to the field of acrylic structural adhesives, in particular to a fast-positioning two-component acrylic structural adhesive. Background technique [0002] The second-generation acrylic structural adhesive can be cured at room temperature, the operation process is simple, and the bonding range is wide. It is suitable for bonding most metal and non-metal materials. The surface treatment requirements are not strict, and even oil surface bonding is possible. 100% solid content, low curing shrinkage, high peel strength, impact resistance and good weather resistance strength, structural bonding halogen-free metal structural adhesive. Because of its solvent-free and halogen-free structural adhesive, it is widely used in the bonding and fixing of electronic assembly, handheld products, communication equipment, automobile manufacturing, rail transit, elevators, ships, mobile phone / notebook casings and tablet computers. In recent years, wi...

Claims

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Application Information

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IPC IPC(8): C09J4/06C09J4/02C09J11/04C08G59/66C08G59/50
CPCC08G59/50C08G59/66C09J4/06C09J11/04
Inventor 孙少芳李峰贺国新张利文
Owner YANTAI SEAYU NEW MATERIALS CORP LTD
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