Graphene heat dissipation coating and graphene heat dissipation material for aluminum electrolytic capacitor, and preparation methods thereof
A technology of aluminum electrolytic capacitors and heat-dissipating coatings, which is applied in the direction of anti-corrosion coatings, polyester coatings, epoxy resin coatings, etc., can solve problems such as easy scratches, achieve good electrical insulation performance, strong adhesion, and ensure insulation Effect
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preparation example Construction
[0069] The above-mentioned preparation method of the graphene heat-dissipating coating for aluminum electrolytic capacitor comprises the following steps:
[0070] A prepares the bottom graphene heat dissipation coating:
[0071] Adding the modified graphene oxide powder into the polyester resin, and dispersing evenly, to obtain the feed liquid 1;
[0072] After mixing the rheological additive, dispersant and solvent uniformly, the feed solution 2 is obtained;
[0073] Add feed liquid 1 into feed liquid 2, mix evenly, and perform sand milling or ball milling to obtain feed liquid 3;
[0074] Add silicon carbide and a coupling agent to the feed liquid 3, and after mixing evenly, perform sand milling or ball milling to obtain the bottom graphene heat dissipation coating;
[0075] B prepares the surface layer graphene heat dissipation coating:
[0076] Adding the modified graphene oxide powder into the epoxy resin, and dispersing evenly, to obtain the feed liquid 4;
[0077] A...
specific Embodiment
[0093] The raw materials used in the examples are all commercially available.
[0094] The molecular weight of epoxy resin is 500-3500; the molecular weight of polyester resin is 5000-35000.
[0095] The coupling agent is silane coupling agent KH550.
[0096] The length of silicon carbide is 20-50um.
[0097] The rheological additive is BYK-410.
[0098] The dispersant is MT-415UV dispersant.
[0099] The solvent is toluene or xylene.
[0100] Graphene oxide is a graphene oxide dispersion prepared by an improved hummers method. The graphene oxide dispersion has a sheet diameter of 1-50 μm, and more than 80% of them are within 3 layers.
Embodiment 1
[0102] The specific operation steps are as follows:
[0103] A graphene heat dissipation coating for aluminum electrolytic capacitors
[0104] Prepare 1kg of bottom graphene heat dissipation coating and top layer graphene heat dissipation coating respectively
[0105] Raw material preparation (according to weight percentage):
[0106] The underlying graphene heat dissipation coating includes: 65% polyester resin, 1% modified graphene oxide powder, 1% silane coupling agent KH550, 6% silicon carbide, 1% BYK-410 rheology additive, 2% MT- 415UV dispersant and 24% xylene solvent;
[0107] The surface graphene heat dissipation coating includes: 55% epoxy resin, 1.5% modified graphene oxide powder, 1.5% silane coupling agent KH550, 8% silicon carbide, 1% BYK-410 rheology additive, 2% MT -415UV dispersant and 31% xylene solvent.
[0108] Preparation of paint:
[0109] a prepare the bottom graphene heat dissipation coating:
[0110] (1) After the graphene oxide dispersion prepare...
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