Preparation method of white carbon black/natural rubber composite material
A technology of natural rubber and composite materials, applied in the field of silica/natural rubber composite material preparation, can solve problems such as affecting the health of operators, affecting the performance of rubber products, affecting the performance of rubber products, etc. Performance and dynamic mechanical properties improvement, the effect of solving the effect of additives and filler residues
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Embodiment 1
[0018] The preparation method of the silica / natural rubber composite material involved in this embodiment is the self-gel method, and the process includes four steps of preparing an aqueous solution of silica, preparing an aqueous solution of auxiliary agents, preparing self-gel and dehydrating and drying:
[0019] (1) Preparation of white carbon black aqueous solution: add 40 parts by mass of SiO in No. 1 beaker 2 (silicon dioxide), 5 parts by mass of liquid Si69 (silane coupling agent) solution and deionized water are mixed with 25wt% white carbon black aqueous solution, and the white carbon black aqueous solution is placed in an ultrasonic oscillator with a frequency of 1000 Hz for ultrasonic 10min, Stir once at 5 minutes, and place it in a planetary ball mill for secondary crushing and grinding for 4 hours;
[0020] (2) Preparation of auxiliary agent aqueous solution: add 20 parts by mass of SiO in No. 2 beaker 2 (silicon dioxide), 2 parts by mass of 4020 (antiaging agent...
Embodiment 2
[0024]This embodiment relates to the comprehensive performance test of the silica / natural rubber composite vulcanized rubber. The silica / natural rubber composite prepared by the dry method, the acid flocculation method and the self-gelling method are prepared into the rubber, wherein , the preparation process of the self-gelling rubber compound is as follows: put the silica / natural rubber composite material in an internal mixer at a temperature of 100°C and mix it at a speed of 90r / min for 6min30s, and then mix it at a temperature of 145°C The rubber is discharged to obtain the mixed rubber, and the mixed rubber is placed in an open mill, and at the same time, 1 mass part of S (sulfur) and 1.2 mass parts of CZ (N-cyclohexyl-2-benzothiazole sulfenamide) are added Start the training to obtain the rubber material; carry out the mechanical performance test on the three rubber materials respectively, and the results are as follows: the results are as follows:
[0025]
[0026] ...
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