Resin composition
A technology of resin composition and compound, applied in the direction of epoxy resin coating, coating, etc., can solve the problems of cost and productivity, and achieve the effect of low linear thermal expansion coefficient and excellent flexibility
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[0148] Examples of solvents that can be used in the preparation of component (C) include N,N-dimethylacetamide, N,N-diethylacetamide, N,N-dimethylformamide, and N-methyl -2-pyrrolidone and other amide solvents; ketone solvents such as acetone, methyl ethyl ketone (MEK) and cyclohexanone; ester solvents such as γ-butyrolactone; hydrocarbon systems such as cyclohexane and methylcyclohexane Solvent. In addition, in the preparation of the component (C), if necessary, an imidization catalyst, an azeotropic dehydration solvent, an acid catalyst, etc. can be used. As the imidization catalyst, for example, triethylamine, triisopropylamine, triethylenediamine, N-methylpyrrolidine, N-ethylpyrrolidine, N,N-dimethyl-4 -Tertiary amines such as aminopyridine and pyridine. Examples of the azeotropic dehydration solvent include toluene, xylene, and ethylcyclohexane. As an acid catalyst, acetic anhydride etc. are mentioned, for example. The usage amount of imidization catalyst, azeotropic d...
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[0249] Example
[0250] Hereinafter, the present invention will be specifically explained through examples. The present invention is not limited by these examples. It should be noted that, hereinafter, for "parts" and "%" indicating amounts, unless otherwise clearly stated, "parts by mass" and "% by mass" are represented respectively.
Example Embodiment
[0251]
[0252] Into a 500ml separable flask equipped with a nitrogen introduction tube and a stirring device, 9.13g of 4-aminobenzoic acid 5-amino-1,1'-biphenyl-2-yl ester (compound of formula (1'')) 30 mmol), 4,4'-(4,4'-isopropylidene diphenoxy) bisphthalic dianhydride 15.61g (30 mmol), N-methyl-2-pyrrolidone 94.64g , 0.47g (6mmol) of pyridine, 10g of toluene, under nitrogen atmosphere, at 180°C, while venting toluene out of the system in the middle, the imidization reaction was carried out for 4 hours to obtain a polyimide containing Polyimide solution of resin 1 (non-volatile content 20% by mass). In the polyimide solution, precipitation of the synthesized polyimide resin 1 was not observed.
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