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Reflective film, its preparation method and application

A reflective film and sputtering power technology, which is applied in the field of reflective film, can solve the problems of economic benefit decline, film layer peeling, poor adhesion, etc., and achieve the effect of simple and efficient preparation method, reducing holes or gaps, and reducing raw material costs

Active Publication Date: 2022-03-08
NINGBO RADI COOL ADVANCED ENERGY TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

On the one hand, the reflective film prepared by this preparation method still cannot effectively eliminate the problems of oxidation and vulcanization; on the other hand, adding a multi-layer dielectric film will complicate the process, and will also cause a series of problems such as film peeling and poor adhesion. other questions
Silver alloy itself has good oxidation resistance and sulfuration resistance, but silver alloy often contains precious metals, and the entire film layer is sputtered with silver alloy targets, which will cause a significant increase in manufacturing costs and a significant decline in economic benefits

Method used

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  • Reflective film, its preparation method and application
  • Reflective film, its preparation method and application
  • Reflective film, its preparation method and application

Examples

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preparation example Construction

[0040] see figure 1 , the present invention provides a reflective film 100 and a preparation method thereof. The preparation method is not only simple and efficient, but can reduce manufacturing costs, and the prepared reflective film 100 can effectively solve the problem of yellow edge oxidation on the edge of the reflective film 100 .

[0041] Specifically, the preparation method comprises the following steps:

[0042] (1) Provide a substrate 10 and a first target, and make the first target form a first layer 20 on the surface of the substrate 10 under vacuum and a first sputtering power;

[0043] (2) Provide a second target material, and make the second target material form the second layer 30 on the side of the first layer 20 away from the substrate 10 under vacuum and second sputtering power, wherein the The second target material includes a first section, a first middle section and a second section, the first middle section is arranged between the first section and the ...

Embodiment 1

[0086] In the chamber of the winding magnetron sputtering coating machine, the 80 μm PET film substrate is placed on the unwinding roller of the unwinding chamber, and is wound on the winding roller; at the same time, the first target, the second target The material and the third target are sequentially placed on the cathode target positions corresponding to the adjacent first chamber, the second chamber and the third chamber; the first target, the second target and the third target are placed on the The distance between the surface of the PET film substrate is adjusted to 10cm; close all chamber doors, turn on the backing pump and molecular pump in turn, and wait until the vacuum degree of the chamber reaches 5×10 -4 Pa, fill the process gas to the process vacuum, open the cathode and the driving roller to start the coating, and control the winding speed at 8m / min. During the magnetron sputtering deposition coating, the temperature in all chambers was kept constant at 15°C. ...

Embodiment 2

[0095] This embodiment is basically the same as Embodiment 1, the only difference is:

[0096] The substrate used is a 100 μm PEN film substrate; the distances from the first target, the second target and the third target to the surface of the PET film substrate are all adjusted to 8cm; the winding speed is controlled at 8m / min; During the sputter deposition of the coating, the temperature in all chambers was kept constant at 0°C, respectively.

[0097] The first sputtering power is 6kW, the first target material is AgPd alloy, and the mass fraction of Pd metal in the AgPd alloy is 1%, and the thickness of the first layer is 20nm.

[0098] The second sputtering power is 40kW, the material of the first segment in the second target is AgRn alloy, and the mass fraction of Rn metal in the AgRn alloy is 3%, and the length of the AgRn alloy accounts for 1 / 20 of the length of the second target, The material of the second section is AgCo alloy, and the mass fraction of Co metal in th...

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Abstract

The invention relates to a reflective film, its preparation method and application. The preparation method comprises: making a first target material form a first layer on the surface of a substrate under vacuum and a first sputtering power; using a second sputtering power to The second target material forms a second layer on the surface of the first layer, the second target material includes a first section, a first middle section and a second section, the first middle section is arranged between the first section and the second section, and The material of the first middle section is silver; the third target is made to form a third layer on the surface of the second layer under the third sputtering power, and a reflective film is produced. In the present invention, three kinds of targets are used to sequentially form films on the surface of the substrate to form a box-like protective structure, and wrap the pure silver reflective film in the middle of the box-shaped structure so that the pure silver reflective film does not External water and oxygen contact can effectively solve the problem of yellow edge oxidation on the edge of the reflective film. In addition, the preparation method is simple and efficient, and saves manufacturing costs.

Description

technical field [0001] The invention relates to the technical field of reflective films, in particular to a reflective film, its preparation method and application. Background technique [0002] The reflective film is mostly sputtered with pure silver target, but the oxidation resistance and sulfuration resistance of pure silver are poor. Using pure silver target for coating will cause the problem of yellow edge oxidation on the edge of the film surface, and reduce the reflectivity of the pure silver film and Adhesion to the substrate. [0003] At present, the way to prevent the oxidation of the yellow edge of the reflective film is to add a multi-layer dielectric protective layer on the pure silver film or use a silver alloy target coating. On the one hand, the reflective film prepared by this preparation method still cannot effectively eliminate the problems of oxidation and vulcanization; on the other hand, adding a multi-layer dielectric film will complicate the process...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C14/35C23C14/34C23C14/14C23C14/08C23C14/06G02B1/14G02B5/08F25B23/00
CPCC23C14/3407C23C14/35C23C14/14C23C14/0641C23C14/0617C23C14/083C23C14/081C23C14/0652C23C14/086C23C14/08G02B5/0833G02B5/085G02B1/14F25B23/00
Inventor 徐绍禹翟怀伦赵锦玲颜毓雷尹铮杰王明辉其他发明人请求不公开姓名
Owner NINGBO RADI COOL ADVANCED ENERGY TECH CO LTD