A rbcl/bacl 2 Mixed aerosol and method for preparing magnesium-based metal semi-solid slurry
A technology of semi-solid slurry and magnesium-based metals, which is applied in the fields of aerosol preparation, chemical instruments and methods, colloid chemistry, etc. It can solve the problems that are rarely reported in the application, and achieve simple and reliable equipment, improved surface tension, and stable process Effect
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Embodiment 1
[0033] In this example, this method is used to prepare a 3Kg-AZ91 magnesium alloy semi-solid slurry.
[0034] A RbCl / BaCl 2 The preparation method of mixed aerosol comprises the following steps:
[0035] Chemically pure RbCl (rubidium chloride) and BaCl 2 (Barium chloride) powder by mass ratio RbCl: BaCl 2 = 2:3 for mixing, as an aerosol solute;
[0036] Add the prepared aerosol solute into a 50L high-pressure gas tank, and the mass of the added aerosol solute is RbCl / BaCl 2 80% of the mixed aerosol mass;
[0037] Then chemically pure argon at room temperature and 14.5MPa is compressed into a high-pressure gas tank for mixing to form RbCl / BaCl 2 The mixed aerosol is stored until use.
[0038] Using the above RbCl / BaCl 2 The method for preparing magnesium-based metal semi-solid slurry by mixing aerosol, the schematic diagram of its preparation process is as follows figure 2 As shown, it specifically includes the following steps:
[0039] The smelted 645°C AZ91 magnesi...
Embodiment 2
[0042] In this example, this method is used to prepare a 3Kg-AZ91 magnesium alloy semi-solid slurry.
[0043] Chemically pure RbCl (rubidium chloride) and BaCl 2 (Barium chloride) powder by mass ratio RbCl: BaCl 2 =2:3 is mixed, as aerosol solute;
[0044] Add the prepared aerosol solute into a 50L high-pressure gas tank, and the mass of the added aerosol solute is RbCl / BaCl 2 Mixed aerosols account for 82% of the mass;
[0045] Then chemically pure helium at room temperature and 14.5MPa is compressed into a high-pressure gas tank for mixing to form RbCl / BaCl 2 The mixed aerosol is stored until use.
[0046] Using the above RbCl / BaCl 2 The method for preparing magnesium-based metal semi-solid slurry by mixing aerosol, the schematic diagram of its preparation process is as follows image 3 shown, including the following steps:
[0047] The AZ91 alloy is heated to 650°C, and the obtained AZ91 alloy melt 4 is placed in the mold 6; the AZ91 alloy melt 4 is poured into the l...
Embodiment 3
[0050] In this example, this method is used to prepare a 3Kg-AM60 magnesium alloy semi-solid slurry.
[0051] Chemically pure RbCl (rubidium chloride) and BaCl 2 (Barium chloride) powder by mass ratio RbCl: BaCl 2 =2:3 is mixed, as aerosol solute;
[0052] Add the prepared aerosol solute into a 50L high-pressure resistant gas tank, wherein the amount of aerosol solute added is 85% of the mass of the aerosol;
[0053] Argon and helium with an equal volume ratio at room temperature and 14.5MPa are then compressed into a high-pressure gas tank for mixing to form RbCl / BaCl 2 The mixed aerosol is stored until use.
[0054] Using the above RbCl / BaCl 2 The method for preparing magnesium-based metal semi-solid slurry by mixing aerosol, the schematic diagram of its preparation process is as follows Figure 4 shown, including the following steps:
[0055] Weigh 3Kg of AM60 magnesium alloy with deoxidized layer and heat it to 630°C, place the obtained AM60 magnesium alloy melt 4 in...
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