Low-thermal conductivity composite foam material and preparation method thereof
A technology of composite foam and low thermal conductivity, which is applied in the field of preparation of composite foam materials with low thermal conductivity, can solve the problems of poor dimensional stability of aerogel materials, limited operability and application, low mechanical strength, etc., and achieves good insulation. Thermal insulation properties and mechanical properties, improved mechanical properties, the effect of uniform porosity
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Embodiment 1
[0032] A composite foam material with low thermal conductivity, consisting of a resin-based foam matrix and aerogel, wherein the ratio of the mass parts of the resin-based foam matrix to the aerogel is 1:0.5, and the aerogel is silica aerogel .
[0033] The method for preparing the composite foam material with low thermal conductivity is characterized in that it comprises the following specific steps:
[0034] (1) Resin, hollow microspheres, thermally expanded microspheres, curing agent, accelerator, coupling agent, toughening agent, and flame retardant are 100:20:2:4:2:1:3 in mass parts: Mix evenly at a ratio of 5 to obtain a mixed slurry;
[0035] (2) Filling the mixed slurry into a mold for molding, and curing to obtain a resin-based foam matrix;
[0036] (3) Mix the silicon source, ethanol, water, and catalyst uniformly to obtain a silica sol, wherein the molar ratio of the silicon source, ethanol, water, and catalyst is 1:5:5:0.003;
[0037] (4) The silica sol prepared in step (3...
Embodiment 2
[0046] A composite foam material with low thermal conductivity, composed of a resin-based foam matrix and aerogel, wherein the mass ratio of the resin-based foam matrix to the aerogel is 1:1, and the aerogel is silica aerogel .
[0047] The preparation method of the aforementioned low thermal conductivity composite foam material includes the following specific steps:
[0048] (1) Resin, hollow microspheres, thermal expansion microspheres, curing agent, accelerator, coupling agent, toughening agent, and flame retardant are 100:30:5:10:3:2:5 in mass parts: Mix evenly at a ratio of 10 to obtain a mixed slurry;
[0049] (2) Filling the mixed slurry into a mold for molding, and curing to obtain a resin-based foam matrix;
[0050] (3) Mix the silicon source, ethanol, water, and the catalyst to obtain a silica sol, wherein the molar ratio of the silicon source, ethanol, water and the catalyst is 1:10:5:0.004;
[0051] (4) The silica sol prepared in step (3) is impregnated with the resin-base...
Embodiment 3
[0060] A composite foam material with low thermal conductivity, composed of a resin-based foam matrix and aerogel, wherein the ratio of the mass parts of the resin-based foam matrix to aerogel is 1:5, and the aerogel is silica aerogel .
[0061] The preparation method of the aforementioned low thermal conductivity composite foam material includes the following specific steps:
[0062] (1) Resin, hollow microspheres, thermally expandable microspheres, curing agent, accelerator, coupling agent, toughening agent, and flame retardant are 100:40:1:4:2:2:3 in mass parts: Mix evenly at a ratio of 20 to obtain a mixed slurry;
[0063] (2) Filling the mixed slurry into a mold for molding, and curing to obtain a resin-based foam matrix;
[0064] (3) Mix the silicon source, ethanol, water, and the catalyst to obtain a silica sol, wherein the molar ratio of the silicon source, ethanol, water, and catalyst is 1:7:9:0.0015;
[0065] (4) The silica sol prepared in step (3) is impregnated with the re...
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