Electroslag remelting premelted slag for improving purity of GH4169 alloy return scraps and preparing method

A GH4169, electroslag remelting technology, applied in the field of pure smelting of superalloys, can solve the problems of high production cost and low utilization rate of returned materials, and achieve the effect of improving purity, obvious innovation and practicability

Active Publication Date: 2020-07-07
AVIC BEIJING INST OF AERONAUTICAL MATERIALS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0009] Aiming at the problems of low utilization rate and high production cost of high-quality deformed superalloy GH4169 used in the field of aero-engines, the present invention proposes a pre-melted slag composition and preparation method for electroslag remelting that improves the purity of GH4169 returned materials, which will help To improve the metallurgical quality level and performance stability of deformed superalloys in my country, and meet the needs of reducing costs and improving purity in the field of superalloy return materials

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0043] Embodiment 1: Pre-melted slag is batched: the composition ratio is CaF 2 : 50%+CaO: 23%+Al 2 o 3 : 20%+MgO: 3%+TiO 2 : 2%+MgF 2 : 2%, moisture in pre-slag at 600°C: 0.03%; SiO 2 : 0.4%; C: 0.02%; P: 0.01%; S: 0.004%; put the above raw materials weighed and proportioned according to the weight percentage requirements of the components into the ball mill for ball milling, and the ball milling time is 2 hours; The good raw material is put into the electric arc furnace, and the electricity is sent, and the graphite electrode is used to heat up and melt the raw material until it is completely melted. Sampling and X-ray fluorescence spectrometer is used for component inspection, and the composition of the pre-slag is required to be within the design composition range; after the slag is completely melted, the liquid slag is poured into a steel cooling plate with a water cooling device at the bottom to cool; the cooling The final pre-melted slag is poured into the crusher ...

Embodiment 2

[0045] Pre-melted slag for batching: the composition ratio is CaF 2 : 43%+CaO: 21%+Al 2 o 3 : 20%+MgO: 4%+TiO 2 : 2%+MgF 2 : 1%, moisture in pre-slag at 600°C: 0.06%; SiO 2 : 0.3%; C: 0.02%; P: 0.01%; S: 0.005%; put the above raw materials weighed and proportioned according to the weight percentage of the components into a ball mill for ball milling, and the ball milling time is 3 hours; The good raw material is put into the electric arc furnace, and the electricity is sent, and the graphite electrode is used to heat up and melt the raw material until it is completely melted. Sampling and X-ray fluorescence spectrometer is used for component inspection, and the composition of the pre-slag is required to be within the design composition range; after the slag is completely melted, the liquid slag is poured into a steel cooling plate with a water cooling device at the bottom to cool; the cooling The final pre-melted slag is poured into the crusher for crushing, and the parti...

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Abstract

The invention belongs to the technical field of high-temperature alloy purifying smelting and relates to an electroslag remelting premelted slag for improving the purity of GH4169 alloy return scrapsand a preparing method. According to the ranges of composition proportions of the premelted slag, CaF2 accounts for 40-55%, CaO accounts for 20-25%, Al2O3 accounts for 18-22%, MgO accounts for 3-6%, TiO2 accounts for 2-3%, and MgF2 accounts for 1-2%; and in the premelted slag at 600 DEG C or lower, moisture is smaller than or equal to 0.06%, SiO2 is smaller than or equal to 0.5%, C is smaller thanor equal to 0.03%, P is smaller than or equal to 0.01%, and S is smaller than or equal to 0.005%. Prepared ceramic materials are subjected to ball milling mixing, smelting through an electric arc furnace, quick cooling and crushing screening, then dried for 2-3 h at the high temperature of 950 DEG C +/-20 DEG C and finally sealed and packaged under the protection of the inert gas (Ar). The premelted slag can ensure the internal metallurgical quality and the surface quality of GH4169 alloy return scrap ingots for aircraft engines, the alloy purity is high, and the premelted slag has the advantages of energy conservation and environmental friendliness, and has wide market prospects and application value.

Description

technical field [0001] The invention belongs to the technical field of pure smelting of high-temperature alloys, and relates to pre-melted slag for electroslag remelting and a preparation method thereof for improving the purity of GH4169 alloy returned materials. Background technique [0002] The background technology of this project is high-temperature alloy electroslag remelting technology and high-temperature alloy return material recovery and reuse technology. [0003] With the rapid development of my country's aerospace, gas turbine, nuclear power and other industries, the use of superalloy materials is increasing. However, superalloy parts have many processing procedures, long manufacturing process, and low material utilization rate. For example, the weight of superalloy final parts is usually only 30% of the total weight of the original input metal materials (weight percentage, the same below), and even some are only about 10% %, the rest are in the form of scraps su...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22B9/18C22C1/06C22C19/05
CPCC22B9/18C22C1/06C22C19/056
Inventor 张勇韦康贾崇林王涛肖程波
Owner AVIC BEIJING INST OF AERONAUTICAL MATERIALS
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