A composition with hypoglycemic effect and its application
A technology for lowering blood sugar and composition, applied in the field of compositions with hypoglycemic effect, can solve the problems of high dosage and limited hypoglycemic effect, and achieve the effects of reducing drug resistance and reducing dosage
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Embodiment 1
[0030]A composition with hypoglycemic effect, the active ingredients of which are hesperetin and geranin; the mass concentration ratio of hesperetin and geranin in the composition is 3:10.
[0031]Test of inhibiting α-glucosidase activity in vitro when the mass concentration ratio of hesperetin and geraniol is 3∶10
[0032]1.1 Reagents: α-glucosidase (α-glucosidase, Sigma, 750U), 4-nitrophenyl-α-D-glucopyranoside (pNPG, TOKYO Chemica Industry Co., LTD), Acarbose , TOKYO ChemicaIndustry Co., LTD), corosolic acid, Na2HPO4, NaH2PO4.
[0033]Experimental instrument: Microplate reader TECAN infinite M200 PRO (Teacan Group Ltd., Swizerland).
[0034]1.2 Experimental steps:
[0035]1.2.1 Preparation of drug solution: first prepare hesperetin, geraniol, acarbose and corosolic acid with dimethyl sulfoxide (DMSO) into a mother liquor of 10mg / mL, and use ultrapure water, Na2HPO4And NaH2PO4Prepare 67 mmol / mL phosphate buffer (PBS, pH=6.8), prepare 5 mmol / mL pNPG solution with PBS, and prepare 0.25 U / mL α-gluc...
Embodiment 2
[0067]A composition with hypoglycemic effect, the active ingredients of which are hesperetin and geranin; the mass concentration ratio of hesperetin and geranin in the composition is 6:10.
[0068]Test of inhibiting α-glucosidase activity in vitro when the mass concentration ratio of hesperetin and geraniol is 6∶10
[0069]2.1 Reagents: α-glucosidase (α-glucosidase, Sigma, 750U), 4-nitrophenyl-α-D-glucopyranoside (pNPG, TOKYO Chemica Industry Co., LTD), Acarbose , TOKYO ChemicaIndustry Co., LTD), corosolic acid, Na2HPO4, NaH2PO4.
[0070]Experimental instrument: Microplate reader TECAN infinite M200 PRO (Teacan Group Ltd., Swizerland).
[0071]2.2 Experimental steps:
[0072]2.2.1 Preparation of drug solution: first prepare hesperetin, geraniol, acarbose and corosolic acid with dimethyl sulfoxide (DMSO) into a mother liquor of 10mg / mL, and use ultrapure water, Na2HPO4And NaH2PO4Prepare 67 mmol / mL phosphate buffer (PBS, pH=6.8), prepare 5 mmol / mL pNPG solution with PBS, and prepare 0.25 U / mL α-gluc...
Embodiment 3
[0103]A composition with hypoglycemic effect, the active ingredients of which are hesperetin and geranin; the mass concentration ratio of hesperetin and geranin in the composition is 8:10.
[0104]Test of inhibiting α-glucosidase activity in vitro when the mass concentration ratio of hesperetin and geraniol is 8∶10
[0105]3.1 Reagents: α-glucosidase (α-glucosidase, Sigma, 750U), 4-nitrophenyl-α-D-glucopyranoside (pNPG, TOKYO Chemica Industry Co., LTD), Acarbose , TOKYO ChemicaIndustry Co., LTD), corosolic acid, Na2HPO4, NaH2PO4.
[0106]Experimental instrument: Microplate reader TECAN infinite M200 PRO (Teacan Group Ltd., Swizerland).
[0107]3.2 Experimental steps:
[0108]3.2.1 Preparation of drug solution: first prepare hesperetin, geraniol, acarbose and corosolic acid with dimethyl sulfoxide (DMSO) into a mother liquor of 10mg / mL, and use ultrapure water, Na2HPO4And NaH2PO4Prepare 67 mmol / mL phosphate buffer (PBS, pH=6.8), prepare 5 mmol / mL pNPG solution with PBS, and prepare 0.25 U / mL α-gluc...
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