Method for rapidly preparing flexible battery by using carbon nanotube continuum
A carbon nanotube, flexible battery technology, applied in battery electrodes, climate sustainability, sustainable manufacturing/processing, etc., can solve the problems of low electrode strength, poor flexibility, hindering performance improvement, etc. The effect of reducing electrochemical impedance and improving rate performance
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Embodiment 1
[0014] Preparation of carbon nanotube-coated electrode (positive electrode): the positive electrode active material is lithium cobaltate. Weigh 1.5 g of the positive electrode active material and disperse it in 50 ml of ethanol solution, ultrasonic power 400 W, ultrasonic dispersion for 30 min and then set aside; spread a 100*300 mm collection paper on the collection roller, and wet it with ethanol solution, and put the carbon The nanotube continuum is drawn onto the collecting paper and shrinks continuously to form a thin film. After depositing a 0.5 μm thick carbon nanotube film on the collecting paper, the dispersed positive electrode active material is sprayed on the carbon nanotube film through an atomizer. Repeat once in 1 min. After all the active material mixture is sprayed, continue to cover the surface with a 0.5 μm thick carbon nanotube film to form an electrode with carbon nanotube-coated active material. The active material loading in the electrode is controlled at...
Embodiment 2
[0020] Preparation of carbon nanotube-coated electrode (positive electrode): the positive electrode active material is lithium iron phosphate. Weigh 4.5 g of the positive electrode active material and disperse it in 150 ml of ethanol solution, ultrasonic power 600 W, ultrasonic dispersion for 25 min and then set aside; spread 100*300 mm collection paper on the collection roller, and wet it with ethanol solution, and put the carbon The nanotube continuum is introduced onto the collecting paper and shrinks into a thin film continuously. After the carbon nanotube film with a thickness of 1.5 μm is deposited on the collecting paper, the dispersed positive electrode active material is sprayed on the carbon nanotube film through an atomizer. Repeat once in 2 min. After all the active material mixture is sprayed, continue to cover the surface with a 1.5 μm thick carbon nanotube film to form an electrode with carbon nanotube-coated active material. The active material loading in the el...
Embodiment 3
[0026] Preparation of carbon nanotube-coated electrode (positive electrode): the positive electrode active material is lithium cobalt oxide. Weigh 3 g of the positive electrode active material and disperse it in 100 ml of ethanol solution, use ultrasonic power of 550 W, and ultrasonically disperse for 20 min before use; spread a 100*300 mm collection paper on the collection roller, and wet it with ethanol solution, The nanotube continuum is drawn onto the collecting paper and shrinks continuously to form a thin film. After depositing a 1 μm thick carbon nanotube film on the collecting paper, the dispersed positive electrode active material is sprayed on the carbon nanotube film through an atomizer. Repeat once in 1.5 min. After all the active material mixture is sprayed, continue to cover the surface with a 1 μm thick carbon nanotube film to form an electrode with carbon nanotube-coated active material. The active material loading in the electrode is controlled at 10 mg / cm 2 ...
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