Amino-containing organic compound and application thereof
A technology of organic compounds and amine groups, applied in the field of organic compounds containing amine groups, can solve problems such as differences, achieve high glass transition temperature, improve optoelectronic properties, and optimize structure.
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Embodiment 1
[0060] Embodiment 1: the synthesis of compound 7:
[0061]
[0062] In a 250ml three-neck flask, under the protection of nitrogen, add 0.01mol raw material 1-1, 0.012mol raw material 2-1, 150ml toluene and stir to mix, then add 5×10 -5 molPd 2 (dba) 3 , 5×10 -5 mol P(t-Bu) 3 , 0.03mol sodium tert-butoxide, heated to 105°C, refluxed for 24 hours, sampling plate, showed no bromide remaining, the reaction was complete; naturally cooled to room temperature, filtered, the filtrate was rotary evaporated to no fraction, passed through a neutral silica gel column , obtain target product compound 7; HPLC purity 99.51%, yield 68.7%; Elemental analysis structure (molecular formula C 43 h 33 N): theoretical value C, 91.61; H, 5.90; N, 2.48; test value: C, 91.63; H, 5.89; N, 2.47. ESI-MS (m / z) (M+): The theoretical value is 563.74, and the measured value is 563.78.
[0063] The following compounds were prepared in the same manner as in Example 1 (the raw materials used were all p...
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