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High-temperature-resistant tough degradable temporary plugging agent and preparation method thereof

A technology of temporary plugging agent and high temperature resistance, which is applied in the field of high temperature resistant toughness degradable temporary plugging agent and its preparation, which can solve the problems of difficult pressure bearing effect, poor thermal stability, loss of strength, etc., to prevent rapid collapse and improve thermal stability performance, and the effect of improving the crystallization speed

Pending Publication Date: 2020-09-22
北京金圣奥能源技术有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For example, the invention patent with the publication number CN109233773A discloses a non-linear self-degradable temporary plugging agent for multi-cluster fracturing reconstruction in a stage. The temporary plugging agent is made of polyglycolide, polylactide-glycolide and polyvinyl alcohol The composed mixture is used as the main body, supplemented with initiator, lubricant, molding agent, reinforcing agent, and degradation-promoting agent, and is made by extruding and granulating; although the temporary plugging agent disclosed in this patent does not stick to water at normal temperature, it is beneficial to pump injection, and the dissolution rate and time can show a nonlinear relationship at the reservoir temperature, but its rigidity is relatively high and its toughness is poor, which is not conducive to the mutual accumulation of temporary plugging particles to form a stable low-permeability plugging with a pressure-bearing effect layer, and its thermal stability is poor under high temperature conditions, it is easy to lose strength quickly, and it is difficult to maintain a stable pressure bearing effect

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] A high-temperature-resistant toughness degradable temporary plugging agent, prepared from the following components and raw materials in parts by weight: 80-90 parts of polyglycolic acid, 10-20 parts of polyester elastomer, and 1-5 parts of plasticizer , 2-8 parts of compatibilizer, 0.5-3 parts of antioxidant, 0.5-3 parts of nucleating agent, 0.2-1 part of crystallization accelerator, 0.4-2 parts of hydrolysis regulator, 5-15 parts of lubricant and thermal stability 0.5-2 doses.

[0032] According to the above content, the polyglycolic acid is end-capped polyglycolic acid.

[0033] According to the above content, the end-capping treatment refers to the end-capping treatment by adding an end-capping agent in the volatilization stage of the glycolic acid monomer in the final stage of the polymerization to form polyglycolic acid.

[0034] According to the above content, the end-capping agent is benzoic acid, and the addition amount of the end-capping agent is 0.5-1 wt% of ...

Embodiment 2

[0044] A high-temperature-resistant toughness degradable temporary plugging agent, prepared from the following components and raw materials in parts by weight: 80 parts of polyglycolic acid, 10 parts of polyester elastomer, 1 part of plasticizer, 2 parts of compatibilizer , 0.5 parts of antioxidant, 0.5 part of nucleating agent, 0.2 part of crystallization accelerator, 0.4 part of hydrolysis regulator, 5 parts of lubricant and 0.4 part of heat stabilizer. All the other configuration steps, methods, principles, and ingredient structure are the same as in Example 1.

Embodiment 3

[0046] A high-temperature-resistant toughness degradable temporary plugging agent, prepared from the following components and raw materials in parts by weight: 85 parts of polyglycolic acid, 15 parts of polyester elastomer, 3 parts of plasticizer, and 4 parts of compatibilizer , 2 parts of antioxidant, 2 parts of nucleating agent, 0.5 part of crystallization accelerator, 1 part of hydrolysis regulator, 10 parts of lubricant and 1.5 parts of heat stabilizer. All the other configuration steps, methods, principles, and ingredient structure are the same as in Example 1.

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PUM

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Abstract

The invention relates to a high-temperature-resistant tough degradable temporary plugging agent and a preparation method thereof. The temporary plugging agent is prepared from the following componentsand raw materials in parts by weight: 80 to 90 parts of polyglycolic acid, 10 to 20 parts of polyester elastomer, 1 to 5 parts of plasticizer, 2 to 8 parts of compatilizer, 0.5 to 3 parts of antioxidant, 0.5 to 3 parts of nucleating agent, 0.2 to 1 part of crystallization promoter, 0.4 to 2 parts of hydrolysis regulator, 5 to 15 parts of lubricant and 0.5 to 2 parts of heat stabilizer. The temporary plugging agent has good high-temperature resistance and toughness, can still keep enough mechanical strength under the high-temperature condition, can be automatically degraded and easily removedafter being used, does not influence an underground reservoir, can effectively improve the construction efficiency of underground temporary plugging steering fracturing, and reduces the construction cost.

Description

technical field [0001] The invention belongs to the technical field of petroleum and natural gas exploitation, and relates to a degradable temporary plugging agent with high temperature resistance and toughness and a preparation method thereof. Background technique [0002] As we all know, oil and gas resources such as oil or natural gas are produced through the exploitation of wells (oil wells or gas wells, sometimes collectively referred to as "pit wells") containing porous and permeable underground layers. However, in recent years, with the continuous exploitation of oil and gas fields, the quality of reservoirs will decline year by year. For this reason, relevant oil and gas producers often use reservoir fracturing to improve the permeability of underground reservoirs, so as to continue to effectively remove these Exploitation of oil and gas resources in underground reservoirs. However, for heterogeneous low-permeability reservoirs characterized by relatively dispersed ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/508C09K8/502
CPCC09K8/5086C09K8/5083C09K8/502
Inventor 冯志强杨波于坤
Owner 北京金圣奥能源技术有限公司
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