Foaming reinforced filling material for coal mine and preparation method thereof
A filling material and foaming technology, which is applied in the field of foaming materials, can solve the problems of difficulty in using inorganic reinforcement materials, small crack width, and unusability, etc., so as to improve the coal recovery rate, meet the safety of use, and increase the foaming ratio. tune effect
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Embodiment 1
[0041] Weigh 500g of sulfoaluminate cement, 370g of fly ash, 8g of calcium stearate, 2g of naphthalenesulfonate formaldehyde polymer, 0.5g of lithium carbonate, 5g of manganese dioxide, and 35g of sodium percarbonate in a powder mixer Mix well and evenly, and prepare the foaming reinforcement filling material for coal mines.
[0042] The above-prepared materials were placed in a stirring tank with a paddle stirrer added with 370 g of water in advance, stirred for 2 minutes to mix evenly, and poured into a mold for foaming and forming.
[0043] It was observed that the material lost fluidity after 4 minutes and solidified after 20 minutes. The finally obtained molded parts do not collapse or crack, and the foaming ratio is 8 times. Using GB / T 17671-1999 cement mortar strength test method (ISO method) to test the compressive strength of the molded parts is 0.8Mpa.
Embodiment 2
[0045] Weigh 500g of sulfoaluminate cement, 8g of quicklime, 300g of ordinary Portland cement, 8g of calcium stearate, 1.9g of naphthalenesulfonate formaldehyde polymer, 0.6g of lithium carbonate, 1g of PVA17-88, and 7.7g of manganese dioxide 1. 20 g of sodium percarbonate was fully mixed in a powder mixer to prepare a foaming reinforcement filling material for coal mines.
[0046]Put the above-prepared material in a mixing tank with a paddle stirrer added with 300g of water in advance, stir for 2 minutes to mix evenly, pour it into a mold for foaming, foaming starts after 10 minutes, and starts to solidify after 20 minutes.
[0047] The molded parts do not collapse or crack, the foaming ratio is 4 times, and the compressive strength is 1.5Mpa.
Embodiment 3
[0049] Weigh 500g of sulfoaluminate cement, 5.7g of quicklime, 150g of ordinary Portland cement, 150g of fly ash, 8g of calcium stearate, 1.5g of naphthalenesulfonate formaldehyde polymer, 0.5g of lithium carbonate, and 1g of PVA17-88 , 7.5 g of manganese dioxide, and 30 g of sodium percarbonate were fully mixed in a powder mixer to prepare a foaming reinforcement filling material for coal mines.
[0050] Put the above-prepared material in a mixing tank with a paddle stirrer added with 300g of water in advance, stir for 2 minutes to mix evenly, pour it into a mold for foaming, foaming starts after 8 minutes, and starts to solidify after 20 minutes.
[0051] The molded parts do not collapse or crack, the foaming ratio is 1.5 times, and the compressive strength is 5.5Mpa.
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