Passivator used for powder zincizing metal workpiece and preparing method and application of passivator
A technology for metal workpieces and powder zinc infiltration, which is applied in the direction of metal material coating process, coating, solid-state diffusion coating, etc., can solve the problems of poor passivation effect, non-environmental protection and corrosion resistance of passivating agents, and achieve passivation Fast speed, good passivation effect, and easy industrialization
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[0027] A preparation method of a passivating agent for powder sherardizing metal workpieces of the present invention comprises the following steps:
[0028] 1) taking water, heating the temperature of the water to 35-45 ° C, taking chromium trichloride, adding it to the water, stirring to obtain a chromium trichloride solution;
[0029] 2) get sodium nitrite, join it in the chromium trichloride solution of step 1) gained, stir, make it dissolve completely, obtain the first solution;
[0030] 3) get cobalt chloride and nickel chloride, join successively in the first solution of step 2) gained, stir, make it dissolve completely, obtain the second solution;
[0031] 4) take ammonium bifluoride, add it to the second solution obtained in step 3), stir to dissolve it completely, and obtain the third solution;
[0032] 5) get hydrogen peroxide, join in the third solution obtained in step 4), stir, make it dissolve completely, obtain the third solution;
[0033] 6) The third solutio...
Embodiment 1
[0041] A preparation method of a passivating agent for powder sherardizing metal workpieces of the present invention comprises the following steps:
[0042] 1) take by weighing raw materials according to the following parts by weight: chromium trichloride 5g, sodium nitrite 10g, nickel chloride 2g, cobalt chloride 5g, ammonium bifluoride 2g, mass concentration is 30% hydrogen peroxide 15mL, water 700mL;
[0043] 2) taking water, heating the temperature of the water to 35°C, taking chromium trichloride, adding it to the water, stirring to obtain a chromium trichloride solution;
[0044] 3) get sodium nitrite, join in the chromium trichloride solution of step 2) gained, stir, make it dissolve completely, obtain the first solution;
[0045] 4) get cobalt chloride and nickel chloride, join successively in the first solution of step 3) gained, stir, make it dissolve completely, obtain the second solution;
[0046] 5) take ammonium bifluoride, add it to the second solution obtained...
Embodiment 2
[0050] A preparation method of a passivating agent for powder sherardizing metal workpieces of the present invention comprises the following steps:
[0051] 1) take by weighing raw materials according to the following parts by weight: chromium trichloride 26g, sodium nitrite 20g, nickel chloride 4g, cobalt chloride 8g, ammonium bifluoride 6g, mass concentration is 30% hydrogen peroxide 25mL, water 700mL;
[0052] 2) taking water, heating the temperature of the water to 45°C, taking chromium trichloride, adding it to the water, stirring to obtain a chromium trichloride solution;
[0053] 3) get sodium nitrite, join in the chromium trichloride solution of step 2) gained, stir, make it dissolve completely, obtain the first solution;
[0054] 4) get cobalt chloride and nickel chloride, join successively in the first solution of step 3) gained, stir, make it dissolve completely, obtain the second solution;
[0055] 5) take ammonium bifluoride, add it to the second solution obtaine...
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