Phospholipid-coated aluminum nanoparticle vaccine adjuvant-delivery system loaded with squalane compound and SARS-CoV2 subunit vaccine
A subunit vaccine and vaccine adjuvant technology, applied in the field of biopharmaceuticals, can solve problems such as strong local irritation, difficult cellular immune response, and inflammatory response at the vaccination site
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Embodiment 1
[0068] Embodiment 1: Construct SPLAN and SCV2 subunit vaccine with SPC / DOTAP / Squalene and aluminum hydroxide nanoparticles
[0069] Take an appropriate amount of lipid materials (SPC and DOTAP) and Squalene (mass ratio of SPC / DOTAP / Squalene = 10:10:1), put them in a pear-shaped flask, add chloroform (the amount used is 3 times the weight of the lipid materials) to dissolve , room temperature, with 90rpm (90 rev / min) rotary evaporation, remove all organic solvents, form SPC / DOTAP / Squalene film.
[0070] According to AN / lipid material (SPC and DOTAP)=10:1 (mass ratio), add the aluminum hydroxide nanoparticle (AN, 1%w / v) aqueous solution (10mM HEPES buffer that contains average particle diameter 80 nanometers) to above-mentioned flask solution, pH=7), and rotated at 120 rpm for 1 hour to fully hydrate the SPC / DOTAP / Squalene film to form SPLAN.
[0071] Then the flask was transferred to a constant temperature electromagnetic stirrer, an electromagnetic stirrer was added, and at r...
Embodiment 2
[0086] Embodiment 2: Construct SPLAN and SCV2 subunit vaccine with SPC / DOTAP / Squalane and alumina nanoparticles
[0087] Take an appropriate amount of lipid materials (SPC and DOTAP) and Squalene (SPC / DOTAP / Squalane=15:10:1, w / w), put them in a pear-shaped flask, add chloroform (3 times the weight of lipid materials) to dissolve, At room temperature, the organic solvent was removed by rotary evaporation at 90 rpm (90 revolutions / minute) to form a SPC / DOTAP / Squalane film.
[0088] According to AN / lipid material (SPC and DOTAP=8:1 (mass ratio), add aluminum oxide nanoparticles (AN, 1% w / v) aqueous solution (10 mM HEPES buffer solution) containing an average particle size of 50 nm to the above flask , pH=7), rotate at 120 rpm for 1 hour to fully hydrate the SPC / DOTAP / Squalane film to form SPLAN.
[0089] Then the flask was transferred to a constant temperature electromagnetic stirrer, an electromagnetic stirrer was added, and at room temperature and 200rpm stirring conditions, a...
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