Manufacturing process of fishing net thread with low cost and good flame retardance
A production process and technology for fishing net threads, which are applied in the manufacture of fire-retardant and flame-retardant filaments, rayon manufacturing, and single-component polyamide rayon filaments, etc. Raw material composition and other issues, to achieve the effect of strong compatibility and binding ability and stability, environmental protection and cost reduction
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Embodiment 1
[0026] Low-cost production process of twine good flame retardancy, comprising the steps of:
[0027] (1) Extraction of waste material:
[0028] . A The scrap nylon twine 66 into the sulfuric acid solution, and then acetic anhydride was added, sonicated well and then stirred, followed by cooling and crystallization, and finally filtered to obtain filtrate A standby;
[0029] . B was added to the filtrate obtained operating a barium sulfate A, mix well before addition of calcium hydroxide and nanofiller, the reaction process after 3h was filtered to obtain the filtrate B backup;
[0030] . C operation b B obtained filtrate by distillation under reduced pressure, to give waste material after the completion of use;
[0031] (2) Nylon 66 wet resin prepared:
[0032] a. The step (1) of waste material obtained with adipic acid, blended with an ethanol solution, after neutralization and a salt precipitated was then filtered, washed alcohol, after the drying process, is configured to 50% m...
Embodiment 2
[0045] Low-cost production process of twine good flame retardancy, comprising the steps of:
[0046] (1) Extraction of waste material:
[0047] . A The scrap nylon twine 66 into the sulfuric acid solution, and then acetic anhydride was added, sonicated well and then stirred, followed by cooling and crystallization, and finally filtered to obtain filtrate A standby;
[0048] . B was added to the filtrate obtained operating a barium sulfate A, mix well before addition of calcium hydroxide and nanofiller, treatment 3.3h the reaction was filtered to obtain the filtrate B backup;
[0049] . C operation b B obtained filtrate by distillation under reduced pressure, to give waste material after the completion of use;
[0050] (2) Nylon 66 wet resin prepared:
[0051] a. The step (1) of waste material obtained with adipic acid, blended with an ethanol solution, after neutralization and a salt precipitated was then filtered, washed alcohol, after the drying process, is configured to 56% of ...
Embodiment 3
[0064] Low-cost production process of twine good flame retardancy, comprising the steps of:
[0065] (1) Extraction of waste material:
[0066] . A The scrap nylon twine 66 into the sulfuric acid solution, and then acetic anhydride was added, sonicated well and then stirred, followed by cooling and crystallization, and finally filtered to obtain filtrate A standby;
[0067] . B was added to the filtrate obtained operating a barium sulfate A, mix well before addition of calcium hydroxide and nanofiller, the reaction process after 3.5h was filtered to obtain the filtrate B backup;
[0068] . C operation b B obtained filtrate by distillation under reduced pressure, to give waste material after the completion of use;
[0069] (2) Nylon 66 wet resin prepared:
[0070] a. The step (1) of waste material obtained with adipic acid, blended with an ethanol solution, after neutralization and a salt precipitated was then filtered, washed alcohol, after the drying process, is configured to 60%...
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