Preparation method of hydrogen storage material

A technology of hydrogen storage materials and sol-gel method, which is applied in the field of preparation of hydrogen storage materials, achieves the effects of strong controllability, lower hydrogen desorption temperature, and strong repeatability

Active Publication Date: 2020-12-25
BEIJING NORMAL UNIVERSITY
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] The present invention aims to solve the problems described above

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  • Preparation method of hydrogen storage material
  • Preparation method of hydrogen storage material
  • Preparation method of hydrogen storage material

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preparation example Construction

[0045] A kind of preparation method of hydrogen storage material of the present invention, comprises the following steps:

[0046] 1S: Ultrasonic cleaning of the porous copper mesh;

[0047] The thickness of the porous copper mesh is 0-2mm, and the mesh number of the copper mesh is 600-1200 mesh

[0048] 2S: Implantation of noble metal ions into the porous copper mesh;

[0049] The metal ion source is selected for implantation, the ion beam current is 0.2-1mA, the pulse width is 20-200μs, the implanted metal is Ag, Au, Pt, etc., the implantation energy is 0-4KeV, and the dose is 1×10 15 -1×10 16 / cm 2 ;

[0050] 3S: Preparation of copper oxide nanowires at high temperature under oxygen atmosphere;

[0051] The temperature for high temperature oxidation in vacuum equipment is 400-750°C, the gas in the vacuum chamber is oxygen gas, the pressure is 0.1-50Pa, the length of copper oxide nanowires is 30-100μm, and the density is 10-50 / μm 2 .

[0052] 4S: copper oxide nanowire...

Embodiment 1

[0058] 1S: Ultrasonic cleaning of the porous copper mesh;

[0059] The thickness of the porous copper mesh is 0-2mm, and the mesh number of the copper mesh is 800 mesh

[0060] 2S: Implantation of noble metal ions into the porous copper mesh;

[0061] The metal ion source was selected for implantation, the ion beam current was 0.5mA, the pulse width was 50μs, the implanted metal was Ag, the implantation energy was 2KeV, and the dose was 1×10 15 -1×10 16 / cm 2 ;

[0062] 3S: Preparation of copper oxide nanowires at high temperature under oxygen atmosphere;

[0063] When the vacuum equipment is oxidized at high temperature, the temperature is 650°C, the gas in the vacuum chamber is oxygen gas, and the pressure is 10Pa. The length of the prepared copper oxide nanowire is 30 μm, and the density is 30 / μm 2 .

[0064] 4S: copper oxide nanowires wrapped in titanium oxide by sol-gel method;

[0065] A wrapped titanium dioxide film is prepared by a sol-gel method, the solution i...

Embodiment 2

[0069] 1S: Ultrasonic cleaning of the porous copper mesh;

[0070] The thickness of the porous copper mesh is 0-2mm, and the mesh number of the copper mesh is 1000 mesh

[0071] 2S: Implantation of noble metal ions into the porous copper mesh;

[0072] The metal ion source was selected for implantation, the ion beam current was 0.6mA, the pulse width was 50μs, the implanted metal was Ag, the implantation energy was 3KeV, and the dose was 1×10 15 -1×10 16 / cm 2 ;

[0073] 3S: Preparation of copper oxide nanowires at high temperature under oxygen atmosphere;

[0074] The temperature of vacuum equipment is 700°C during high temperature oxidation, the gas in the vacuum chamber is oxygen gas, the pressure is 20Pa, the length of copper oxide nanowires is 40μm, and the density is 30 / μm 2 .

[0075] 4S: copper oxide nanowires wrapped in titanium oxide by sol-gel method;

[0076] A wrapped titanium dioxide film is prepared by a sol-gel method, the solution includes tetrabutyl ti...

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Abstract

The invention discloses a preparation method of a nano hydrogen storage material. The preparation method comprises the following steps of 1S, carrying out ultrasonic cleaning on porous copper; 2S, preparing a copper oxide nanowire through high-temperature oxidation in an oxygen atmosphere; 3S, preparing a titanium oxide coated copper oxide nanowire by a sol-gel method; and 4S, performing magnesiumdeposition on the nanowire by using a magnetic filtering technology. The method is based on the high-temperature oxidation, ion implantation, the sol-gel method and the magnetic filtration depositionmethod, and can be used for conveniently absorbing and desorbing hydrogen to form an ultra-nano composite structure; hydrogen absorption material prepared by the method has the characteristics of strong hydrogen absorption capacity, low hydrogen desorption temperature, self-cleaning and the like; and the hydrogen absorption material disclosed by the invention has an important application prospectin the aspect of hydrogen energy.

Description

technical field [0001] The invention belongs to the field of new energy, and in particular relates to a preparation method of a hydrogen storage material. Background technique [0002] With the development of industry and the improvement of people's material living standards, the demand for energy is also increasing day by day. Since the energy used in recent decades mainly comes from fossil fuels (such as coal, oil and natural gas, etc.), and its use inevitably pollutes the environment, and its reserves are limited, so it is urgent to find renewable green energy. As a green energy and energy carrier with abundant reserves, wide sources and high energy density, hydrogen energy is attracting widespread attention. The utilization of hydrogen energy needs to solve the following three problems: hydrogen production, storage, transportation and application, and the storage and transportation of hydrogen energy is the key to the application of hydrogen energy. Hydrogen exists in ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C28/00C23C14/18C23C14/32C23C14/48C23C14/58C23C18/12
CPCC23C28/322C23C28/345C23C14/48C23C14/5806C23C14/5853C23C18/1254C23C18/1216C23C14/32C23C14/18
Inventor 廖斌欧阳晓平罗军
Owner BEIJING NORMAL UNIVERSITY
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