Unlock instant, AI-driven research and patent intelligence for your innovation.

Preparation method of large-caliber columnar ceramic membrane support body and ceramic membrane product thereof

A ceramic membrane support and large-diameter technology, which is applied in the field of membrane separation, can solve the problems of unfavorable product quality control and large-diameter extrusion products, and achieve the effects of easy extrusion molding and control, reduced permeation resistance, and reduced process difficulty

Pending Publication Date: 2021-01-05
JINGDEZHEN CERAMIC INSTITUTE
View PDF6 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For tubular ceramic membranes with a large diameter such as a diameter exceeding 40mm, only hydraulic extruders can be used to extrude intermittently, which is not conducive to product quality control
However, if screw extrusion is adopted, the diameter of the screw rod of the screw extruder must be doubled to ensure a certain screw compression ratio due to the large diameter of the extruded product. At present, there is no related extrusion equipment.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Preparation method of large-caliber columnar ceramic membrane support body and ceramic membrane product thereof
  • Preparation method of large-caliber columnar ceramic membrane support body and ceramic membrane product thereof
  • Preparation method of large-caliber columnar ceramic membrane support body and ceramic membrane product thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0037] The preparation method of a large-diameter columnar ceramic membrane product in this embodiment is as follows: the separation membrane layer slurry is coated on the inner wall of the raw material liquid channel 3 of the large-diameter columnar ceramic membrane support to form a separation membrane layer, and a large-diameter columnar ceramic membrane product is obtained. Ceramic membrane products.

[0038] Wherein, the preparation method of large diameter columnar ceramic membrane support body is, as figure 1 As shown, the large-diameter (diameter is 60mm) columnar porous channel (180 channels) ceramic membrane is divided symmetrically along the axial direction to form 6 monomers, and each monomer is used as a support unit 1 (see figure 2 ), first adopt extrusion molding to prepare each support body unit 1 respectively, and then splicing and combining to form a columnar structure; the steps are as follows:

[0039] (1) Preparation of support unit 1

[0040] Mix 100kg...

Embodiment 2

[0049] The preparation method of a large-diameter columnar ceramic membrane product in this embodiment differs from Embodiment 1 in that:

[0050] The preparation of the separation membrane layer slurry in this embodiment is as follows: get 10g Dolapix CE-64 and dissolve it in 9kg water, add 1kg of alumina powder with an average particle diameter of 0.2 μm, and then add 30g of polyvinyl alcohol 1750 (polyvinyl alcohol needs to be prepared in advance into a solution with a concentration of 10% by weight), and mixed together under vigorous stirring conditions to obtain a stable suspension slurry.

[0051] In the preparation of the separation membrane layer in this example, the calcination temperature was 1350° C., and the holding time was 2 hours to obtain a separation membrane layer with an average pore diameter of 50 nm, that is, to produce a large-diameter columnar ceramic membrane product.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
particle sizeaaaaaaaaaa
particle sizeaaaaaaaaaa
pore sizeaaaaaaaaaa
Login to View More

Abstract

The invention discloses a preparation method of a large-caliber columnar ceramic membrane support body. The preparation method comprises the following steps: taking a monomer formed by symmetrically and equally dividing a large-caliber columnar ceramic membrane along the axial direction as a support body unit, firstly preparing the support body unit by extrusion molding; and then splicing and combining to form a ceramic membrane structure with a columnar structure and gaps among the support body units as penetrating fluid channels. In addition, the invention further discloses a large-caliber columnar ceramic membrane product and a preparation method thereof. The large-caliber ceramic membrane is formed by dividing the large-caliber ceramic membrane into the small support body units, carrying out extrusion molding and then combining the small support body units so that the process difficulty of preparing the large-caliber ceramic membrane is reduced, and meanwhile, membrane defects arealso avoided. According to the ceramic membrane configuration adopted by the invention, not only is the process of processing the permeation channels in the later period of the ceramic membrane reduced, but also the permeation distance of the permeation liquid at the membrane surface of the middle pore channel of the large-diameter ceramic membrane is greatly reduced, and compared with the existing large-caliber ceramic membrane configuration, the permeation flux of the large-caliber ceramic membrane is effectively improved.

Description

technical field [0001] The invention relates to the technical field of membrane separation, in particular to a preparation method of a columnar ceramic membrane support body and a ceramic membrane product thereof. Background technique [0002] Inorganic ceramic membranes have the advantages of high temperature resistance, solvent resistance, acid and alkali corrosion resistance, high mechanical strength, easy cleaning and regeneration, and have unique technical advantages in chemical, food, pharmaceutical and other fields. At present, the configurations of ceramic membrane products are mainly single tubular, multi-channel tubular, honeycomb tubular and flat plate. Among them, multi-channel ceramic membranes have been widely used in industry due to their easy port sealing and less membrane fouling. However, the disadvantage of multi-channel ceramic membranes is that the membrane area per unit volume is relatively small, resulting in a high proportion of investment in membran...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/10C04B35/14C04B35/46C04B35/48C04B35/565C04B35/622C04B38/06C04B41/87B01D67/00B01D71/02
CPCC04B35/10C04B35/14C04B35/46C04B35/48C04B35/565C04B35/622C04B38/0645C04B41/009C04B41/5031C04B41/87B01D71/027B01D67/0039C04B2235/3217C04B2235/3232C04B2235/3244C04B2235/3418C04B2235/3826C04B2235/5436C04B2235/6021C04B2235/606C04B2235/656C04B2235/6567C04B2235/95C04B41/4535C04B41/0072
Inventor 王霞常启兵郝恩奇何世斌杨柯汪永清
Owner JINGDEZHEN CERAMIC INSTITUTE
Features
  • R&D
  • Intellectual Property
  • Life Sciences
  • Materials
  • Tech Scout
Why Patsnap Eureka
  • Unparalleled Data Quality
  • Higher Quality Content
  • 60% Fewer Hallucinations
Social media
Patsnap Eureka Blog
Learn More