Supercharge Your Innovation With Domain-Expert AI Agents!

Preparation method and application of carbide slag super-early-strength admixture

A technology of calcium carbide slag and admixture, which is applied in the field of building materials, can solve the problems of durability of prefabricated components and the negative impact of later strength development, increase the production cost of concrete prefabricated components, and not involve the application of low solid content carbide slag, etc., to speed up The effect of growth, dense pore structure, and simple application method

Active Publication Date: 2021-01-08
HUBEI UNIV OF TECH
View PDF11 Cites 4 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] (1) Curing concrete with steam at 60°C to 80°C for 8 hours. Although this method can effectively shorten the demoulding time, steam curing consumes a lot of energy, which increases the production cost of concrete prefabricated components, and the crystal growth of hydration products is coarse. The durability of concrete members is very unfavorable
[0004] (2) Adding inorganic early-strength agents to accelerate cement hydration, but inorganic early-strength agents are usually made of industrial raw materials, the cost is high, and ions with smaller atomic radii will be introduced, such as K + 、Na + , Cl - etc., so that the use of inorganic early strength agents is limited, and has a certain negative impact on the durability of prefabricated components and the development of later strength
[0005] (3) Adding nano or submicron nuclei to induce cement hydration through the nucleation effect, which has minimal harm to cement, but the production cost of the nuclei is relatively high
The preparation method has complex procedures, and there are microwave-enhanced calcination and grinding procedures, which consume a lot of energy.
[0009] At present, most of the applications of carbide slag in improving the strength of cement have problems such as complex process and high cost, and there is no application involving low solid content carbide slag, and there is no addition of submicron carbide slag to cement glue in the form of an admixture Concrete materials, to enhance the application of its early strength

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Preparation method and application of carbide slag super-early-strength admixture
  • Preparation method and application of carbide slag super-early-strength admixture
  • Preparation method and application of carbide slag super-early-strength admixture

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0035] The specific embodiment of the preparation method of the calcium carbide slag super-early strength admixture of the present invention will be provided below. In this specific embodiment, the carbide slag used comes from each calcium carbide method to produce acetylene factories, and the wet mill used is a vertical planetary ball mill, including the steps:

[0036] (1) Take 20-60 parts by mass of carbide slag and 0.5-1 part by mass of dispersant, add 80-160 parts by mass of water, mix and stir, and sieve to obtain carbide slag slurry with a particle size of less than 1 mm. The dispersant is used to avoid the aggregation of carbide slag, specifically, triethanolamine and / or diethanolamine can be used. The calcium carbide slag used in the present invention has a solid content of 30% to 95%, and its main mineral component is calcium hydroxide, wherein the content of calcium oxide is greater than 75%, the content of silicon oxide is greater than 3%, and the content of aluminu...

Embodiment 1

[0048] The specific steps of this embodiment are as follows:

[0049] (1) Take 35 parts by mass of carbide slag, 0.8 part by mass of diethanolamine dispersant and 120 parts by mass of water, mix, stir and sieve to obtain a calcium carbide slag slurry with a diameter of less than 1 mm. The solid content of the carbide slag used is 90%.

[0050] (2) Mix the calcium carbide slag slurry with propylene glycol grinding aid, polycarboxylate plasticizer and 300 parts by mass of zirconia balls, and grind them in a wet mill until the median particle size reaches 232nm and the specific surface area is 26560m 2 / kg, sieve the grinding medium to obtain ultrafine slurry of carbide slag. Among them, the dosage of propylene glycol grinding aid is 1‰ of the solid content of carbide slag in the carbide slag slurry, and the dosage of polycarboxylate plasticizer is 17‰ of the solid content of carbide slag in the carbide slag slurry. The ball ratio is 4:1:1.

[0051] (3) Add an anti-agglomeratio...

Embodiment 2

[0055] The specific steps of this embodiment are as follows:

[0056] (1) Take 35 parts by mass of carbide slag, 1 part by mass of diethanolamine dispersant and 90 parts by mass of water, mix, stir and sieve to obtain a carbide slag slurry with a diameter of less than 1 mm, and the solid content of the carbide slag used is 90%.

[0057] (2) Mix the calcium carbide slag slurry with propylene glycol grinding aid, polycarboxylate plasticizer and 300 parts by mass of zirconia balls, and place them in a wet mill to grind until the median particle size reaches 241nm (the specific surface area is 25680mm 2 / kg), and sieve the grinding medium to obtain ultrafine slurry of carbide slag. Among them, the dosage of propylene glycol grinding aid is 1‰ of the solid content of carbide slag in the carbide slag slurry, and the dosage of polycarboxylate plasticizer is 23‰ of the solid content of carbide slag in the carbide slag slurry. The ball ratio is 4:1:1.

[0058] (3) Add an anti-agglome...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
Specific surface areaaaaaaaaaaa
Diameteraaaaaaaaaa
Diameteraaaaaaaaaa
Login to View More

Abstract

The invention discloses a preparation method and application of a carbide slag super-early-strength admixture. The preparation method comprises the following steps: (1) taking 20-60 parts by mass of carbide slag and 0.5-1 part by mass of a dispersant, adding 80-160 parts by mass of water, mixing and stirring, and screening to obtain carbide slag slurry; (2) adding a grinding aid of which the carbide slag solid content in the carbide slag slurry is 0.05-0.15%, a plasticizer of which the carbide slag solid content in the carbide slag slurry is 0.5-2.5% and 300-400 parts by mass of a grinding medium into the carbide slag slurry, grinding in a wet mill, and screening the grinding medium to obtain carbide slag superfine slurry; and (3) adding an anti-agglomeration stabilizer into the carbide slag superfine slurry, and stirring to obtain the carbide slag super-early-strength admixture. According to the invention, the method disclosed by the invention is simple in process, low in energy consumption and low in cost; and after the prepared carbide slag super-early-strength admixture is added into a cement cementing material, the early strength of the cement cementing material can be remarkably enhanced, the later strength is not reduced, and the additional value of carbide slag products is increased.

Description

technical field [0001] The invention belongs to the technical field of building materials, and in particular relates to a preparation method and application of a calcium carbide slag super early strength admixture. Background technique [0002] With the development of my country's construction industry, early-strength concrete is playing an increasingly important role in fields such as emergency repair and construction projects, production of concrete prefabricated components, and road and bridge construction. In order to improve the early strength of concrete, the methods commonly used at present are as follows: [0003] (1) Curing concrete with steam at 60°C to 80°C for 8 hours. Although this method can effectively shorten the demoulding time, steam curing consumes a lot of energy, which increases the production cost of concrete prefabricated components, and the crystal growth of hydration products is coarse. The durability of concrete members is very unfavorable. [000...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): C04B24/28C04B28/04C04B103/10
CPCC04B40/0039C04B28/04C04B2103/10C04B2201/50C04B2201/52C04B18/0481C04B24/122C04B24/026C04B24/283C04B24/166C04B22/10C04B24/18Y02W30/91
Inventor 杨进曾景义范梦甜谢云轩贺行洋苏英郑正旗李玉博王迎斌江波
Owner HUBEI UNIV OF TECH
Features
  • R&D
  • Intellectual Property
  • Life Sciences
  • Materials
  • Tech Scout
Why Patsnap Eureka
  • Unparalleled Data Quality
  • Higher Quality Content
  • 60% Fewer Hallucinations
Social media
Patsnap Eureka Blog
Learn More