LED lamp sheet capable of displaying three-dimensional picture, and processing technology thereof
A processing technology and light film technology, which is applied to the photoengraving process of the pattern surface, the display device, the illuminated mark, etc., can solve the problems of inability to display multiple pictures, increase the cost, and complicated the replacement of pictures, and achieve the durability of the pattern. Excellent, improved adhesion, reasonable process design effect
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Embodiment 1
[0044] Step 1: Take hydroxypropyl carboxymethylcellulose, dissolve it in deionized water, stir for 5 minutes, slowly add europium trichloride dropwise, continue stirring for 10 minutes, adjust the pH to 8, and then place it at a temperature of 70°C and a microwave power of 800W Under the conditions of 10 min, dialyzed, and dried at 80°C, the ultraviolet fluorescent material was obtained.
[0045] Step 2: Take formaldehyde, zinc acetate and p-tert-butylphenol, heat up to 70°C under nitrogen atmosphere, mix and stir for 2 hours, then slowly add sodium hydroxide solution dropwise, continue stirring for 20 minutes, then react at 80°C for 2 hours, add n-butanol, continue to react for 30min, wash, remove the organic solvent by rotary evaporation in vacuum, and cool to obtain the modified resin.
[0046] Step 3: Take the modified resin and additives, stir at 35°C for 30 minutes, then add dispersant and UV fluorescent material, continue to stir for 20 minutes, then add wetting agent a...
Embodiment 2
[0057] Step 1: Take hydroxypropyl carboxymethyl cellulose, dissolve it in deionized water, stir for 7 minutes, slowly add europium trichloride dropwise, continue stirring for 12 minutes, adjust the pH to 8, and then place it at a temperature of 72°C and a microwave power of 850W Under the conditions of 12 min, dialyzed, and dried at 85°C, the ultraviolet fluorescent material was obtained.
[0058] Step 2: Take formaldehyde, zinc acetate and p-tert-butylphenol, heat up to 72°C under nitrogen atmosphere, mix and stir for 2.3 hours, then slowly add sodium hydroxide solution dropwise, continue stirring for 25 minutes, then react at 85°C for 2.5 hours , add n-butanol, continue to react for 35min, wash, remove the organic solvent by vacuum rotary evaporation, cool to obtain the modified resin.
[0059] Step 3: Take modified resin and additives, stir at 38°C for 35 minutes, then add dispersant and UV fluorescent material, continue stirring for 25 minutes, then add wetting agent and d...
Embodiment 3
[0070] Step 1: Take hydroxypropyl carboxymethylcellulose, dissolve it in deionized water, stir for 8 minutes, slowly add europium trichloride dropwise, continue stirring for 15 minutes, adjust the pH to 9, and then place it at a temperature of 75°C and a microwave power of 900W Under the conditions of 15 min, dialyzed, and dried at 90°C, the ultraviolet fluorescent material was obtained.
[0071] Step 2: Take formaldehyde, zinc acetate and p-tert-butylphenol, heat up to 75°C under nitrogen atmosphere, mix and stir for 2.5h, then slowly add sodium hydroxide solution dropwise, continue stirring for 30min, then react at 90°C for 3h, Add n-butanol, continue the reaction for 40 minutes, wash, remove the organic solvent by vacuum rotary evaporation, and cool to obtain the modified resin.
[0072] Step 3: Take modified resin and additives, stir at 40°C for 40 minutes, then add dispersant and UV fluorescent material, continue to stir for 30 minutes, then add wetting agent and diluent,...
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