Preparation method of carbon dioxide activated paulownia wood powder composite PVC building template
A carbon dioxide, building template technology, applied in the direction of manufacturing tools, wood treatment, impregnating wood, etc., to achieve the effect of increasing bonding performance, improving overall stability, and improving heat-resistant dimensional stability.
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[0028] A carbon dioxide activated paulownia powder composite PVC building formwork preparation method, comprising the following steps:
[0029] (1) Paulownia flour pretreatment:
[0030] Evenly disperse paulownia powder into the ethanol solution, stir evenly, then add ethylenediamine and citric acid to the ethanol solution, adjust the temperature to 55-60°C, keep warm in a water bath, stir for 2 hours, then filter and wash with water until Neutral, dried to constant weight to obtain pretreated paulownia powder;
[0031] Ethylenediamine
[0032] Ethylenediamine, referred to as EDA, the chemical formula is C 2 h 8 N 2 , is a typical fatty diamine, which is colorless or light yellow oily or watery transparent liquid, which produces smoke in the air, has an ammonia-like smell, and is hygroscopic. The molecular weight is 60.10, the melting point is 8.5°C, and the spontaneous ignition point is 385°C. Belongs to alkaline substances, easily soluble in water, ethanol, slightly so...
Embodiment 1
[0062] A carbon dioxide activated paulownia powder composite PVC building formwork preparation method, comprising the following steps:
[0063] (1) Paulownia flour pretreatment:
[0064] Evenly disperse paulownia powder into the ethanol solution, stir evenly, then add ethylenediamine and citric acid to the ethanol solution, adjust the temperature to 55°C, keep warm in a water bath, stir for 2 hours, then filter, wash with water until neutral , and dried to constant weight to obtain pretreated paulownia powder; the mass fraction of the ethanol solution is 20%; the mixing mass ratio of the paulownia powder and ethanol solution is 1:6. The mixing weight ratio of the ethylenediamine, citric acid and ethanol solution is: 1.2:0.3:45.
[0065] (2) Carbon dioxide activation treatment:
[0066] Divide the pretreated paulownia powder into two parts ab, add a part of pretreated paulownia powder into the gasification furnace, then pass in nitrogen gas, exhaust the air in the gasificatio...
Embodiment 2
[0072] A carbon dioxide activated paulownia powder composite PVC building formwork preparation method, comprising the following steps:
[0073] (1) Paulownia flour pretreatment:
[0074] Evenly disperse paulownia powder into the ethanol solution, stir evenly, then add ethylenediamine and citric acid to the ethanol solution, adjust the temperature to 60°C, keep warm in a water bath, stir for 2 hours, then filter, wash with water until neutral , dried to constant weight to obtain pretreated paulownia powder; the mass fraction of the ethanol solution is 20%; the mixing mass ratio of the paulownia powder and ethanol solution is 1:8. The mixing weight ratio of the ethylenediamine, citric acid and ethanol solution is 2:0.5:50.
[0075] (2) Carbon dioxide activation treatment:
[0076] Divide the pretreated paulownia powder into two parts ab, add a part of pretreated paulownia powder into the gasifier, then pass in nitrogen gas, exhaust the air in the gasifier, then adjust the temp...
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