A preparation method of an optical composite film with both diffusion and reflection functions
An optical composite film and functional technology, applied in optics, optical components, optical components, etc., can solve the problems of uneven light distribution, limited brightness of backlight modules, etc., achieve excellent mechanical and optical properties, light weight, low The effect of production costs
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Embodiment 1
[0017] Embodiment 1, a method for preparing an optical composite film with both diffusion and reflection functions, is characterized in that it comprises the following steps:
[0018] A. Ultrasonically mix the fiber with a sulfuric acid solution with a mass percentage of 40% at a mass volume ratio of 1:80g / ml to obtain solution A, react at 90°C for 5 hours, and then add ammonia water and mass percentage to solution A The 60% tetraisopropanone titanate solution continued to react for 5 hours. After the reaction, it was centrifuged and washed with ethanol, and dried in an oven at 70°C to obtain cellulose / titanium dioxide core-shell spherical diffusion particles. Among them, mechanically pulverized polyester staple fibers, the length of the mechanically pulverized polyester staple fibers is controlled between 1-3mm.
[0019] B. Melting high-density polyethylene and polymethacrylic resin with a mass ratio of 3:1g / ml on a roller mill at 170°C, adding titanium dioxide particles for ...
Embodiment 2
[0021] Embodiment 2, a method for preparing an optical composite film with both diffusion and reflection functions, is characterized in that it comprises the following steps:
[0022] A. Ultrasonically mix the fiber with a sulfuric acid solution with a mass percentage of 40% at a mass volume ratio of 1:50g / ml to obtain solution A, react at 80°C for 6 hours, and then add ammonia water and mass percentage to solution A The 70% titanium tetrachloride solution continued to react for 4 hours, after the reaction was completed, it was centrifuged and washed with ethanol, and dried in an oven at 75°C to obtain cellulose / titanium dioxide core-shell spherical diffusion particles. Among them, mechanically pulverized polyester staple fibers, the length of the mechanically pulverized polyester staple fibers is controlled between 1-3mm.
[0023] B. Melt high-density polyethylene and polystyrene with a mass ratio of 3:1.2g / ml on a roller mill at 180°C, add silica particles to blend, the tota...
Embodiment 3
[0025] Embodiment three, a kind of preparation method of the optical composite film with diffusion and reflection function, is characterized in that comprising the following steps:
[0026] A. Ultrasonically mix the fiber with a sulfuric acid solution with a mass percentage of 40% at a mass volume ratio of 1:100g / ml to obtain solution A, react at 60°C for 4.5h, and then add ammonia water and mass percentage to solution A The titanium tetrabromide solution with a content of 50% continued to react for 8 hours. After the reaction, it was centrifuged and washed with ethanol, and dried in an oven at 65°C to obtain cellulose / titanium dioxide core-shell spherical diffusion particles. Among them, mechanically pulverized polyester staple fibers, the length of the mechanically pulverized polyester staple fibers is controlled between 1-3mm.
[0027] B. Melt high-density polyethylene and polymethacrylic resin at a mass ratio of 3:0.5g / ml on a roller mill at 160°C, add titanium dioxide par...
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