High-thermal-conductivity organosilicone gel sheet and preparation method thereof
A silicone gel sheet and high thermal conductivity technology, applied in the field of high thermal conductivity silicone gel sheet and its preparation, can solve the problems of insufficient strength, reduced thermal conductivity, increased production cost, etc., to ensure quality and performance stability, Efficient thermal conductivity and long service life
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[0052] The embodiment of the present invention also provides a method for preparing a high thermal conductivity silicone gel sheet, which is characterized in that it includes the following steps:
[0053] 1) Preparation of side chain polysiloxane containing silicon hydrogen group loaded with thermally conductive filler
[0054] 1.1) Pour the thermally conductive filler into toluene, stir under heating in an oil bath at 50°C to 80°C; then add side-chain vinyl polysiloxane coupling agent and stir; then add deionized water and stir to initiate side-chain vinyl polysiloxane The oxane coupling agent is hydrolyzed and coated on the surface of the thermally conductive filler; after the hydrolysis is completed, filter, and take the filtered particles of the side chain vinyl polysiloxane coupling agent coated with the thermally conductive filler, and wash them with deionized water and absolute ethanol in turn. Washing, and then placing the particles in a blast drying oven for blast dry...
Embodiment 1
[0067] The preparation of silicone gel sheet comprises the following specific steps:
[0068] 1) Preparation of side chain polysiloxane containing silicon hydrogen group loaded with thermally conductive filler
[0069] 1.1) Weigh 13g of thermally conductive filler, pour it into 100mL of toluene, heat it in an oil bath at 60°C, and stir it with a high-speed stirrer at a speed of 1200rpm / min for 3min; then add 10g of side chain vinyl polysiloxane coupling agent and stir 5min; then, add 1.8g of deionized water and stir for 8min to initiate the hydrolysis of the side chain vinyl polysiloxane coupling agent, thereby forming a coating on the surface of the thermally conductive filler. After the reaction, filter, and take the obtained side-chain vinyl polysiloxane-coated thermally conductive filler particles and wash them three times with 30 ml of deionized water, and then three times with 30 ml of ethanol. Subsequently, the particles were placed in a blast drying oven at 60° C. for...
Embodiment 2
[0082] The preparation of silicone gel sheet comprises the following specific steps:
[0083] 1) Preparation of side chain polysiloxane containing silicon hydrogen group loaded with thermally conductive filler
[0084] 1.1) Weigh 18g of thermally conductive filler, pour it into 100mL of toluene, heat it in an oil bath at 80°C, and stir it with a high-speed stirrer at a speed of 1000rpm / min for 5min; then add 10g of side chain vinyl polysiloxane coupling agent and stir 5min; then, add 1.8g of deionized water and stir for 10min to initiate the hydrolysis of the side chain vinyl polysiloxane coupling agent, thereby forming a coating on the surface of the thermally conductive filler. After the reaction, filter, and take the obtained side-chain vinyl polysiloxane-coated thermally conductive filler particles and wash them three times with 30 ml of deionized water, and then three times with 30 ml of ethanol. Then the particles were air-dried in a 70° C. air-drying oven for 12 hours....
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Abstract
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