Photochromic composition of hyper-branched polyurethane vinyl ether, product and preparation method
A polyurethane vinyl ether and photochromic technology, applied in the field of optical films, can solve the problems of large cost burden, waste of discolored powder, easy to appear panda eye vision, etc., and achieve the effects of improving solvent resistance and increasing crosslinking density.
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Embodiment 11
[0044]Add 10g PEG400 to the container, vacuumize at 120°C for 1 hour, cool down to 60°C, add 16.67g IPDI, 55g ethyl acetate and 0.2g DBTDL, heat up to 70°C and keep stirring for 2 hours, cool down to 60°C, slowly drop 1.02g glycerol, heat up to 70°C and keep stirring for 2 hours, cool down to 60°C, slowly add 0.76g pentaerythritol dropwise, heat up to 70°C and keep stirring for 2 hours, test that the NCO content is 2.25%, add 0.02g MEHQ and 5.2g 4-Hydroxybutyl vinyl ether, heat up to 80°C and keep stirring for 2 hours, then add 3.5g midnight gray and 3.5g misty gray, heat up to 90°C and keep stirring for 1 hour, finally add 0.1g BYK1790, 0.1g BYK333, 5.46g PETMP , 0.02gBHT, 0.02g Tinuvin 329, mixed uniformly to obtain a photochromic composition of hyperbranched polyurethane vinyl ether, the refractive index is 1.554. Spray the photochromic coating composition on the surface of the PC lens, rotate at 800rpm for 20 seconds, and then irradiate with a 300W infrared lamp for 2 minu...
Embodiment 12
[0046] Add 10g PEG400 to the container, vacuumize at 120°C for 2 hours, cool down to 60°C, add 16.67g IPDI, 55g ethyl acetate and 0.2g DBTDL, heat up to 70°C and keep stirring for 2 hours, cool down to 60°C, slowly drop 1.02g glycerol, heat up to 70°C and keep stirring for 2 hours, cool down to 60°C, slowly add 0.76g pentaerythritol dropwise, heat up to 70°C and keep stirring for 2 hours, test that the NCO content is 2.25%, add 0.02g MEHQ and 5.2g 4-Hydroxybutyl vinyl ether, heat up to 80°C and keep stirring for 2 hours, then add 3.5g midnight gray and 3.5g misty gray, heat up to 90°C and keep stirring for 1 hour, finally add 0.1g BYK1790, 0.1g BYK333, 5.46g PETMP , 0.02gBHT, 0.02g Tinuvin 329, mixed uniformly to obtain a photochromic composition of hyperbranched polyurethane vinyl ether, the refractive index is 1.554. Spray the photochromic coating composition on the surface of the PC lens, rotate at 800rpm for 20 seconds, and then irradiate with a 300W infrared lamp for 2 mi...
Embodiment 21
[0049] Add 10g PEG600 to the container, vacuumize at 120°C for 1 hour, cool down to 60°C, add 16.67g IPDI, 51.2g ethyl acetate and 0.2g DBTDL, heat up to 70°C and keep stirring for 2 hours, cool down to 60°C, slowly Add 1.19g of glycerol dropwise, heat up to 70°C and keep stirring for 2 hours, cool down to 60°C, slowly add 0.66 pentaerythritol dropwise, heat up to 70°C and keep stirring for 2 hours, test that the NCO content is 3.0%, add 0.02g MEHQ and 6.79 g 4-hydroxybutyl vinyl ether, heat up to 80°C and keep stirring for 2 hours, then add 3.5g midnight gray and 3.5g misty gray, heat up to 90°C and keep stirring for 1 hour, finally add 0.1g BYK1790, 0.1g BYK333, 6.5 gPETMP, 0.02gBHT, and 0.02g Tinuvin 329 were uniformly mixed to obtain a photochromic composition of hyperbranched polyurethane vinyl ether, with a refractive index of 1.554. Spray the photochromic coating composition on the surface of the PC lens, rotate at 800rpm for 20 seconds, and then irradiate with a 300W i...
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