Red yeast rice extract modified protein/cellulose composite fiber and preparation method thereof
A composite fiber and extract technology, applied in the direction of cellulose/protein conjugated artificial filament, fiber chemical characteristics, wet spinning method, etc., can solve the problems of poor washing resistance, easy protein loss, and washing resistance, etc., to achieve Effect of improving washing resistance
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Embodiment 1
[0034] A red yeast rice extract modified protein / cellulose composite fiber whose specification is 1.33dtex*38mm is prepared as follows:
[0035] 1. Preparation of Red Yeast Extract Modified Protein Micropowder Dispersion
[0036] Protein micropowder is wool protein micropowder, particle size D90 = 1.968 μm, red yeast extract (Xi'an Shangcheng Biotechnology Co., Ltd., wherein the mass content of monacolin-K is 3%), according to red yeast extract: protein micropowder = Mix at a mass ratio of 1:5, add it to deionized water, and prepare a red yeast rice extract / protein micropowder dispersion with a mass fraction of protein micropowder of 10%, adjust the pH to 2 with acetic acid, heat up to 70°C, and agitator speed Stir at 400r / min to ensure uniform adsorption, keep warm for 30min, cool down to 20°C, add sodium sulfite to adjust the pH to neutral, emulsify with a high-shear emulsifying homogenizer (LR-100L) at a speed of 1000r / min, and emulsify for 30min , choose the filter materi...
Embodiment 2
[0044] A red yeast rice extract modified protein / cellulose composite fiber whose specification is 1.56dtex*38mm is prepared as follows:
[0045] 1. Preparation of Red Yeast Extract Modified Protein Micropowder Dispersion
[0046] Protein micropowder is silk protein micropowder, particle size D90=1.825μm, red yeast extract (Xi'an Shangcheng Biotechnology Co., Ltd., wherein the mass content of monacolin-K is 3%), according to red yeast extract: protein micropowder= Mix at a mass ratio of 1:5, add it to deionized water, and prepare a red yeast rice extract / protein micropowder dispersion with a protein micropowder mass fraction of 15.0%, adjust the pH to 3 with dilute hydrochloric acid, heat up to 75°C, and stir Stir at a speed of 400r / min to ensure uniform adsorption, keep warm for 40min, cool down to 15°C, add sodium hydroxide to adjust the pH to neutral, and emulsify with a high-shear emulsifying homogenizer (LR-100L) at a speed of 1250r / min. The emulsification time is 20min, ...
Embodiment 3
[0054] A red yeast rice extract modified protein / cellulose composite fiber whose specification is 1.67dtex*38mm is prepared as follows:
[0055] 1. Preparation of Red Yeast Extract Modified Protein Micropowder Dispersion
[0056] Protein micropowder is feather protein micropowder, particle size D90=1.562μm, red yeast extract (Xi'an Shangcheng Biotechnology Co., Ltd., wherein the mass content of monacolin-K is 3%), according to red yeast extract: protein micropowder =1:5 mass ratio to mix, add to deionized water, configure the red yeast rice extract / protein micropowder dispersion with a protein micropowder mass fraction of 20%, adjust the pH to 4 with dilute sulfuric acid, heat up to 80°C, and stir Stir at a speed of 300r / min to ensure uniform adsorption, keep warm for 50min, cool down to 10°C, add sodium sulfite to adjust the pH value to neutral, and emulsify with a high-shear emulsification homogenizer (LR-100L) at a speed of 1500r / min. The time is 10 minutes, and the filter...
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