Anti-influenza virus fabric and preparation method thereof
An anti-influenza virus and fabric technology, applied in textiles and papermaking, liquid-repellent fibers, biochemical fiber treatment, etc., can solve the problems of formaldehyde residues in textiles, production, application and popularization restrictions, hazards, etc. Good performance, high promotion and application value, and simple process
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Embodiment 1
[0026] A kind of preparation method of the anti-influenza virus fabric, is characterized in that, comprises the steps:
[0027] Step S1, preparation of 2,6-diaminopurine / imidazole-4,5-dicarboxylic acid condensation polymer: dissolving 2,6-diaminopurine, imidazole-4,5-dicarboxylic acid and catalyst in a high boiling point solvent Then add the solution to the reaction kettle, replace the air in the kettle with inert gas, react at 110°C for 4 hours under normal pressure, then raise the temperature to 230°C, carry out polycondensation reaction at 300Pa for 10 hours, then cool to room temperature, adjust to normal pressure, precipitated in water, washed the precipitated polycondensate with ethanol for 3 times, and then dried in a vacuum oven at 85°C to constant weight to obtain 2,6-diaminopurine / imidazole-4,5-di Carboxylic acid condensation polymer;
[0028] Step S2, ionized polycondensate: dissolve the 2,6-diaminopurine / imidazole-4,5-dicarboxylic acid polycondensate prepared in s...
Embodiment 2
[0037] A kind of preparation method of the anti-influenza virus fabric, is characterized in that, comprises the steps:
[0038] Step S1, preparation of 2,6-diaminopurine / imidazole-4,5-dicarboxylic acid condensation polymer: dissolving 2,6-diaminopurine, imidazole-4,5-dicarboxylic acid and catalyst in a high boiling point solvent Then add the solution to the reaction kettle, replace the air in the kettle with inert gas, react at 112°C for 4.5 hours under normal pressure, then raise the temperature to 235°C, carry out polycondensation reaction at 350Pa for 11 hours, then cool to room temperature, adjust to normal pressure, precipitated in water, washed the precipitated polycondensate with ethanol 4 times, and then dried in a vacuum oven at 87°C to constant weight to obtain 2,6-diaminopurine / imidazole-4,5-di Carboxylic acid condensation polymer;
[0039] Step S2, ionized polycondensate: dissolve the 2,6-diaminopurine / imidazole-4,5-dicarboxylic acid polycondensate prepared in ste...
Embodiment 3
[0048] A kind of preparation method of the anti-influenza virus fabric, is characterized in that, comprises the steps:
[0049] Step S1, preparation of 2,6-diaminopurine / imidazole-4,5-dicarboxylic acid condensation polymer: dissolving 2,6-diaminopurine, imidazole-4,5-dicarboxylic acid and catalyst in a high boiling point solvent Then add the solution into the reaction kettle, replace the air in the kettle with inert gas, react at 115°C for 5 hours under normal pressure, then raise the temperature to 240°C, carry out polycondensation reaction at 400Pa for 13 hours, then cool to room temperature, adjust to normal pressure, precipitated in water, washed the precipitated polycondensate with ethanol 5 times, and then dried in a vacuum oven at 90°C to constant weight to obtain 2,6-diaminopurine / imidazole-4,5-di Carboxylic acid condensation polymer;
[0050] Step S2, ionized polycondensate: dissolve the 2,6-diaminopurine / imidazole-4,5-dicarboxylic acid polycondensate prepared in ste...
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