Method for improving bonding strength of low-emissivity coating and carbon fiber base material
A low-emissivity coating and carbon fiber substrate technology, which is applied in the fields of carbon fiber, fiber treatment, textiles and paper making, can solve the problems of low-emissivity coating and substrate bond strength reduction, poor mechanical properties, and difficult experimental operations And other issues
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Embodiment 1
[0050] S1: Cleaning the surface of the polyimide-based carbon fiber substrate with an organic solvent;
[0051] S2: Prepare a layer of 5-10 μm silicone resin on the surface of the polyimide-based carbon fiber substrate. After the surface is dry, place it at 200°C and cure for 4 hours to obtain the pretreated polyimide-based carbon fiber substrate;
[0052] S3: Take 60g of organic solvent, add 30g of silicone resin and 30g of flake aluminum powder, stir and disperse at a speed of 600r / min for 10min to obtain a coating;
[0053] S4: Prepare the prepared coating on the pretreated polyimide-based carbon fiber substrate, and then place it at room temperature for 6 hours. After it is surface-dried, cure it at 200°C for 4 hours to obtain a coating thickness of 50~ 60 μm sample.
[0054] Wherein, the organic solvent includes ethyl acetate and butyl acetate, and the mass ratio of ethyl acetate and butyl acetate is 2:1.
Embodiment 2
[0056] S1: heat-treat the polyimide-based carbon fiber substrate in a high-temperature muffle furnace at 500°C for 2 minutes;
[0057] S2: using an organic solvent to clean the surface of the polyimide-based carbon fiber substrate;
[0058] S3: Prepare a layer of 5-10 μm silicone resin on the surface of the polyimide-based carbon fiber substrate. After the surface is dry, place it at 200°C and cure for 4 hours to obtain the pretreated polyimide-based carbon fiber substrate;
[0059] S4: Take 60g of organic solvent, add 30g of silicone resin and 30g of flake aluminum powder, stir and disperse at a speed of 600r / min for 10min to obtain a coating;
[0060] S5: Prepare the prepared coating on the pretreated polyimide-based carbon fiber substrate, and then place it at room temperature for 6 hours. After it is surface-dried, cure it at 200°C for 4 hours to obtain a coating thickness of 50~ 60 μm sample.
[0061] Wherein, the organic solvent includes ethyl acetate and butyl acetat...
Embodiment 3
[0063] S1: heat-treat the polyimide-based carbon fiber substrate in a high-temperature muffle furnace at 500°C for 4 minutes;
[0064] S2: using an organic solvent to clean the surface of the polyimide-based carbon fiber substrate;
[0065] S3: Prepare a layer of 5-10 μm silicone resin on the surface of the polyimide-based carbon fiber substrate. After the surface is dry, place it at 200°C and cure for 4 hours to obtain the pretreated polyimide-based carbon fiber substrate;
[0066] S4: Take 60g of organic solvent, add 30g of silicone resin and 30g of flake aluminum powder, stir and disperse at a speed of 600r / min for 10min to obtain a coating;
[0067] S5: Prepare the prepared coating on the pretreated polyimide-based carbon fiber substrate, and then place it at room temperature for 6 hours. After it is surface-dried, cure it at 200°C for 4 hours to obtain a coating thickness of 50~ 60 μm sample.
[0068] Wherein, the organic solvent includes ethyl acetate and butyl acetat...
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