Nitrogen-sulfur-doped nano-porous carbon material taking sodium alginate as raw material and preparation method of nitrogen-sulfur-doped nano-porous carbon material
A technology of nanoporous carbon and sodium alginate, which is applied in the direction of nanocarbon, nanotechnology, carbon compounds, etc., and can solve problems such as hindering practical application, poor rate performance and cycle stability
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Embodiment 1
[0028] A preparation method of nitrogen-sulfur-doped nanoporous carbon material using sodium alginate as raw material, comprising the following steps:
[0029] 1) Slowly dissolve 2g of sodium alginate powder in 60ml of deionized aqueous solution containing 0.5g of thiourea, continue stirring and heating to form a solution;
[0030] 2) Add 3.91g of calcium acetate to 20ml of deionized water, slowly drop into sodium alginate thiourea solution to form a gel, and keep stirring for 1h;
[0031] 3) The gel in step 2) is freeze-dried and pulverized, and pre-frozen with liquid nitrogen before freeze-drying;
[0032] 4) Activate the sample in step 3) by high-temperature carbonization, and then wash and dry it with hydrochloric acid and deionized water to obtain a nitrogen-sulfur-doped nanoporous carbon material prepared by a freeze-drying assisted carbonization template method, wherein the carbonization temperature is 600 ° C, The drying time is 2 hours, the drying temperature is 60° ...
Embodiment 2
[0038] A preparation method of nitrogen-sulfur-doped nanoporous carbon material using sodium alginate as raw material, comprising the following steps:
[0039] 1) Slowly dissolve 2g of sodium alginate powder in 60ml of deionized aqueous solution containing 0.6g of thiourea, continue stirring and heating to form a solution;
[0040] 2) Add 3.91g of calcium acetate to 20ml of deionized water, slowly drop into sodium alginate thiourea solution to form a gel, and keep stirring for 1 hour;
[0041] 3) The gel in step 2) is freeze-dried and pulverized, and pre-frozen with liquid nitrogen before freeze-drying;
[0042] 4) Activate the sample in step 3) by high-temperature carbonization, and then wash and dry it with hydrochloric acid and deionized water to obtain a nitrogen-sulfur-doped nanoporous carbon material prepared by a freeze-drying assisted carbonization template method, wherein the carbonization temperature is 600 ° C, The drying time is 5 hours, the drying temperature is ...
Embodiment 3
[0045] A preparation method of nitrogen-sulfur-doped nanoporous carbon material using sodium alginate as raw material, comprising the following steps:
[0046] 1) Slowly dissolve 2g of sodium alginate powder in 60ml of deionized aqueous solution containing 0.6g of thiourea, continue stirring and heating to form a solution;
[0047] 2) Add 3.91g of calcium acetate to 20ml of deionized water, slowly drop into sodium alginate thiourea solution to form a gel, and keep stirring for 1 hour;
[0048] 3) The gel in step 2) is freeze-dried and pulverized, and pre-frozen with liquid nitrogen before freeze-drying;
[0049] 4) Activate the sample in step 3) by high-temperature carbonization, and then wash and dry it with hydrochloric acid and deionized water to obtain a nitrogen-sulfur-doped nanoporous carbon material prepared by a freeze-drying assisted carbonization template method, wherein the carbonization temperature is 700 ° C, The drying time is 3 hours, the drying temperature is ...
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