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A kind of preparation method of iodine-containing disinfectant with stable component content

A technology of component content and disinfectant, applied in the direction of disinfectant, botany equipment and methods, medical preparations with non-active ingredients, etc., can solve problems such as aggravating pressure, affecting product disinfection performance, shelf life, and differences

Active Publication Date: 2022-02-25
FOSHAN STANDARD BIO TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

It can be seen from the results that adding substances such as potassium iodate is beneficial to stability, but its stability needs to be further improved
The instability of this iodine disinfectant in the system affects the disinfection performance and shelf life of the product, making the product unable to have the shortcoming of long-term stability, aggravating the pressure during production, stocking, storage and transportation, and causing fluctuations in the disinfection effect What affects the actual disinfecting effect is stability
[0003] When preparing an existing iodine-containing disinfectant, especially when the iodine-containing disinfectant uses iodide (such as potassium iodide) and / or iodate (such as potassium iodate) as a stabilizer, different addition sequences lead to a newly prepared iodine-containing disinfectant The difference in iodine element content in disinfectants leads to differences between different batches and affects industrial production

Method used

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  • A kind of preparation method of iodine-containing disinfectant with stable component content

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preparation example Construction

[0053] In the preparation method of iodine-containing disinfectant of the present invention, select inorganic acid such as sulfuric acid, phosphoric acid etc. as raw material and can obtain stable iodine-containing disinfectant equally according to the reaction described above, but considering the safety of biocompatibility and use etc., Choose organic acids, and further choose carboxylic acids; carboxylic acids are milder in nature and better in biocompatibility than inorganic acids, and iodine can exert a more excellent disinfection and sterilization effect in an acidic medium environment. Therefore carboxylic acid is one of the essential raw materials of the present invention.

[0054] In the description of the present invention, the carboxylic acid preferably has certain water solubility and / or alcohol and / or ester solubility, and is more preferably a carboxylic acid that can undergo esterification reaction under the catalysis of elemental iodine. Such carboxylic acids inc...

Embodiment 1

[0073] 1.1 The raw material components and their consumption amounts for preparing iodine-containing disinfectant are as follows:

[0074] Elemental iodine 2%, anhydrous citric acid 10%, absolute ethanol 88%.

[0075] 1.2 Taking 1000g raw material liquid as an example, the specific preparation method is as follows:

[0076] Take about 300g of absolute ethanol, add 20g of elemental iodine and stir to dissolve to obtain A1 solution; dissolve 100g of citric acid in 400g of absolute ethanol to obtain B1 solution; About 180g of the remaining absolute ethanol is added to the above mixed solution under stirring to obtain a uniform solution, which is the disinfectant raw material solution; the raw material solution is reacted at 70°C under stirring for 12 hours, and then left to cool to obtain a product with long-term component stability. iodine-containing disinfectant.

[0077] 1.3 The composition of elemental iodine and carboxylic acid of this iodine-containing disinfectant after ...

Embodiment 2

[0080] 2.1 The raw material components and their consumption amounts for preparing iodine-containing disinfectant are as follows:

[0081] Elemental iodine 2%, anhydrous citric acid 10%, ethanol 68%, water 20%.

[0082] 2.2 Taking 1000g raw material liquid as an example, the specific preparation method is as follows:

[0083] Take about 300g of absolute ethanol, add 20g of elemental iodine and stir to dissolve to obtain A2 solution; dissolve 100g of citric acid in 380g of absolute ethanol to obtain B2 solution; add B2 solution to A2 solution under stirring, and after fully stirring, Add 200g of water to the above mixed solution under stirring to obtain a uniform solution, which is the raw material solution of the disinfectant; react the raw material solution at 78°C for 15 hours under stirring, and then leave it to cool to obtain an iodine-containing disinfectant with long-term component stability agent.

[0084] 2.3 The composition of elemental iodine and carboxylic acid of...

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Abstract

The invention discloses a preparation method of an iodine-containing disinfectant with stable component content. The method comprises mixing the following raw materials together and reacting at 50-150°C for 5-20 hours, elemental iodine and any one of the following seven Those: (1) carboxylic acid and alcohol (2) carboxylic acid, alcohol and water (3) carboxylic acid, alcohol, carboxylate and water (4) alcohol, carboxylate and water (5) carboxylic acid, carboxylate and water Water (6) Carboxylate and water (7) Carboxylic acid and water. Carboxylic acid, alcohol, water, ester etc. in the iodine-containing disinfectant of the present invention reach equilibrium by reversible esterification and or transesterification under the condition of iodine as catalyzer and / or elemental iodine itself then contains acid, water The disproportionation reaction occurs under the conditions to obtain a stable equilibrium between elemental iodine, iodide ion and iodic acid. The composition of the iodine-containing disinfectant is stable, and the preparation is convenient. After long-term storage (at least two years), the content of iodine, iodide and carboxylic acid remains stable, and has a stable disinfection and sterilization effect.

Description

technical field [0001] The invention belongs to the field of disinfectants, in particular to an iodine-containing disinfectant with stable component content. Background technique [0002] Iodine disinfectants are widely used in various aspects of industrial production and daily life, but the stability of iodine-containing disinfectants has always been a very challenging issue. The main reason for the instability of iodine-containing disinfectants is the reactive nature of simple iodine. In order to stabilize elemental iodine, iodides such as potassium iodide, sodium iodide, etc. are generally added; or acids are added, such as citric acid, salicylic acid, sulfuric acid, phosphoric acid, etc.; Adding iodide and iodate to the system can stabilize the iodine disinfectant to a certain extent, but its content still has obvious changes after long-term storage. For example, in "Influence of complexing agent PVP-K30 on povidone-iodine bactericidal effect and effect improvement" (T...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A01N59/12A01N25/22A01P1/00A61K33/18A61K47/12A61K47/10A61K47/14A61P31/04A61P31/00
CPCA01N59/12A01N25/22A61K33/18A61K47/12A61K47/10A61K47/14A61P31/04A61P31/00
Inventor 王振兴黎剑坤陈艺青刘肖娟符德文谭志坚赵一阳
Owner FOSHAN STANDARD BIO TECH
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