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Precipitation strengthening nickel-based high-temperature alloy laser powder bed melting forming method capable of reducing hot cracks

A nickel-based superalloy and precipitation strengthening technology, applied in the direction of additive processing, can solve the problems of inability to guarantee process stability, small process window, high time cost, and achieve the effect of solving hot cracking problem, high versatility and low cost

Pending Publication Date: 2021-05-25
SOUTH UNIVERSITY OF SCIENCE AND TECHNOLOGY OF CHINA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, for the precipitation-strengthened nickel-based nickel-based superalloys that have been served at high temperatures for a long time and maintain a stable structure, most of the commonly used refiners cannot refine the structure, so they are not suitable for solving the problem of laser powder bed melting. The problem of thermal cracking in forming
[0005] Although some domestic and foreign researches have been carried out to improve the hot cracking of nickel-base superalloys cast by laser powder bed fusion forming method and achieved certain results (see "Selective laser melting of the hard-to-weld IN738LC superalloy: Efforts to mitigate defects and the resultant microstructural and mechanical properties", H.Wang et al., Journal of Alloys and Compounds, Vol. 807), but for the same alloy powder from different powder suppliers or different batches of alloy powder raw materials from the same supplier and different 3D The combination of printing equipment needs to re-explore the appropriate process parameters, and the time cost is high
In addition, for precipitation-strengthened nickel-based superalloys with high content of alloying elements aluminum and titanium, the process window of laser powder bed fusion forming is extremely small, and the process stability cannot be guaranteed.

Method used

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  • Precipitation strengthening nickel-based high-temperature alloy laser powder bed melting forming method capable of reducing hot cracks
  • Precipitation strengthening nickel-based high-temperature alloy laser powder bed melting forming method capable of reducing hot cracks
  • Precipitation strengthening nickel-based high-temperature alloy laser powder bed melting forming method capable of reducing hot cracks

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Effect test

Embodiment 1

[0082] This embodiment provides a method for laser powder bed fusion forming of a precipitation-strengthened nickel-based superalloy that reduces thermal cracking, and the method includes the following steps:

[0083] (1) Mix the IN738LC precipitation-strengthened high-temperature alloy powder with a particle size range of 15-53 μm and a particle size D50 of 30.1 μm with diyttrium trioxide particles with a particle size of 80-130 nm at a mass ratio of 2000:1 to obtain a mixed powder ;

[0084] (2) After evacuating the forming cavity of the laser powder bed melting equipment to 5Pa, after filling argon with a purity of 99.99wt%, the mixed powder is placed in the laser powder bed melting equipment under an argon atmosphere A 30 μm powder layer is formed in the forming cavity of the above, and the powder layer is preheated to a temperature of 200°C;

[0085] (3) The powder layer is fused and formed by laser powder bed under a continuous laser with a beam diameter of 80 μm, a pow...

Embodiment 2

[0088] This embodiment provides a method for laser powder bed fusion forming of a precipitation-strengthened nickel-based superalloy that reduces thermal cracking, and the method includes the following steps:

[0089] (1) Mix the IN738LC precipitation-strengthened high-temperature alloy powder with a particle size range of 10-40 μm and a particle size D50 of 22.3 μm with diyttrium trioxide particles with a particle size of 20-100 nm at a mass ratio of 300:1 to obtain a mixed powder ;

[0090] (2) After evacuating the forming cavity of the laser powder bed melting equipment to 5Pa, after filling helium with a purity of 99.99wt%, the mixed powder is placed in the laser powder bed melting equipment under a helium atmosphere A 10 μm powder layer is formed in the forming cavity of the , and the powder layer is preheated to a temperature of 90°C;

[0091] (3) The powder layer is melted and formed by laser powder bed under a continuous laser with a beam diameter of 75 μm, a power of...

Embodiment 3

[0094] This embodiment provides a method for laser powder bed fusion forming of a precipitation-strengthened nickel-based superalloy that reduces thermal cracking, and the method includes the following steps:

[0095] (1) Mix the IN738LC precipitation-strengthened high-temperature alloy powder with a particle size range of 20-60 μm and a particle size D50 of 33.2 μm with diyttrium trioxide particles with a particle size of 130-280 nm at a mass ratio of 4500:1 to obtain a mixed powder ;

[0096] (2) After evacuating the forming cavity of the laser powder bed melting equipment to 4Pa, after filling argon with a purity of 99.99wt%, the mixed powder is placed in the laser powder bed melting equipment under an argon atmosphere A 60 μm powder layer is formed in the forming cavity of the powder, and the powder layer is preheated to a temperature of 230°C;

[0097] (3) The powder layer is melted and formed by laser powder bed under a continuous laser with a beam diameter of 85 μm, a ...

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Abstract

The invention provides a precipitation strengthening nickel-based high-temperature alloy laser powder bed melting forming method capable of reducing hot cracks. According to the method, rare earth element oxide particles and precipitation strengthening nickel-based high-temperature alloy powder are mixed and then subjected to laser powder bed melting forming, the rare earth element oxide particles and the precipitation strengthening nickel-based high-temperature alloy powder interact under the action of continuous laser, and therefore harmful elements in the original precipitation strengthening nickel-based high-temperature alloy powder can be enriched, segregation of the harmful elements along the crystal boundary is reduced, forming of a liquid film of melt at the final stage of solidification is correspondingly hindered, and the hot cracks are greatly reduced.

Description

technical field [0001] The invention relates to the technical field of mechanical manufacturing, in particular to a method for laser powder bed fusion forming of precipitation-strengthened nickel-based superalloys for reducing thermal cracking. Background technique [0002] The laser powder bed fusion forming method is a commonly used and fastest-growing technology in the field of metal 3D printing in recent years, and has attracted extensive attention from industry and academia. During the forming process, the computer system controls the high-energy laser beam to selectively melt the metal powder, and realizes the rapid forming of complex parts by layer-by-layer accumulation, which has the advantages of material saving and high dimensional accuracy. (such as nickel-based nickel-based superalloys, aluminum alloys, titanium alloys, stainless steel, etc.) [0003] However, there are great technical difficulties in precipitation-strengthened nickel-based superalloy parts that...

Claims

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Application Information

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IPC IPC(8): B22F3/105B33Y10/00C22C1/04C22C19/05
CPCC22C1/0433C22C19/056B33Y10/00
Inventor 郭川朱强徐振李干周阳
Owner SOUTH UNIVERSITY OF SCIENCE AND TECHNOLOGY OF CHINA
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