Bi-component conductive silica gel as well as preparation method and application thereof
A conductive silicone, two-component technology, applied in the field of conductive adhesive, can solve the problem of large heat dissipation, and achieve the effect of improving shielding efficiency, excellent shielding efficiency and good storage stability
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[0041] Preparation Example 1
[0042] A kind of nickel-coated graphite / carbon fiber in the present application is prepared by the following operation steps:
[0043] a. Weigh graphite and carbon fiber in a ratio of 1:3 by weight, and use ultrasonic treatment to mix the two evenly to obtain a graphite / carbon fiber composite material;
[0044] b. Oil removal: the above-mentioned graphite / carbon fiber composite material was deoiled by ultrasonic oscillation with 15wt% NaOH aqueous solution at 54°C for 10min, and the sample was taken out and rinsed with deionized water until neutral;
[0045] c. Roughening: use 10wt% HNO 3 The aqueous solution was coarsened by ultrasonic vibration at 55 °C for 10 min, and the sample was taken out and rinsed with deionized water until neutral;
[0046] d. Sensitization: in 37wt% hydrochloric acid 60mL / L, SnCl 2 ·2H 2 In the sensitizing solution of 0 30g / L, ultrasonically vibrate for 6min, take out the sample, and rinse it with deionized water; ...
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[0050] Preparation Example 2
[0051] The nickel-coated graphite / carbon fiber of Preparation Example 2 is the same as that of Preparation Example 1, except that the same amount of graphite is replaced by flexible graphite.
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[0052] Preparation Example 3
[0053] The fumed silica-titanium dioxide composite powder in this application is prepared by the following operations:
[0054] Pretreatment of fumed silica: Add sodium polyacrylate with 12% total slurry weight, ultrafine grinding for 80min at 23℃, rotating speed 1200r / min, ball-to-material ratio 5.5:1, slurry concentration 2.3% , to obtain the fumed silica after dispersion treatment;
[0055] Pretreatment of titanium dioxide: ultra-fine grinding for 60 minutes at 24°C, rotating speed 1200r / min, ball-to-material ratio of 4:1, and slurry concentration of 50% to obtain dispersed titanium dioxide;
[0056] The treated fumed silica and titanium dioxide are mixed in a weight ratio of 1:0.5, the concentration of the slurry is controlled to be 12%, ultrafine grinding for 40min, and sieving to obtain a silica / titanium dioxide composite material with an average particle size of 1000 meshes .
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