Traditional Chinese medicine composition for treating female animal endometritis and its preparation method and application
A technology of endometritis and composition, which is applied in the field of veterinary medicine, can solve problems such as environmental pollution and single mode of action, unfavorable storage of sanguinarine, and easy resistance to antibiotics, so as to avoid instability and maintain stability Effect
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Embodiment 1
[0032] (1) Take 6 kg of Boluo pods, extract by diafiltration with 0.5% sulfuric acid, then use lye to adjust the solution to a pH value of about 10 to precipitate, obtain a precipitate after filtration, dry the precipitate, and dissolve it with 90% ethanol Sulfuric acid solution was added to precipitate, filtered, and after the precipitate was dried, 113.4 g of the extract was returned, and the percentage of sanguinarine was 40.9% as measured by liquid phase.
[0033] (2) Take 4kg of motherwort medicinal material, extract twice with 10 times of water, and concentrate the combined water extract to about 1.10g / cm 3 , add an equivalent amount of 95% ethanol to carry out alcohol precipitation, recover the alcohol liquid and dry it to obtain 365.8g of Motherwort extract, and the stachydrine hydrochloride is 3.2% as measured by the liquid phase.
[0034] (3) Merge the extract of Boluohui and motherwort, add 110 g of sodium citrate and 33 g of sodium carboxymethylcellulose, mix and p...
Embodiment 2
[0036] (1) Take 7.5kg of boluo pods, extract by diafiltration with 0.5% sulfuric acid, then use lye to adjust the solution to a pH value of about 10 to precipitate, obtain a precipitate after filtration, dry the precipitate, and dissolve it with 90% ethanol Then add sulfuric acid solution to precipitate, filter, and after the precipitate is dried, 141.2 g of the extract will be returned, and the percentage of sanguinarine is 41.2% as measured by liquid phase.
[0037] (2) Take 2.5kg of Motherwort herbs, extract twice with 10 times of water, and concentrate the combined water extracts to about 1.10g / cm 3, add an equivalent amount of 95% ethanol to carry out alcohol precipitation, recover the alcohol liquid and dry it to obtain 230.8g of Motherwort extract, and the stachydrine hydrochloride is 3.4% as measured by the liquid phase.
[0038] (3) Merge the extract of Boluohui and motherwort, add 142g of sodium citrate and 33g of sodium carboxymethylcellulose, mix and pack, and ster...
Embodiment 3
[0040] (1) Take 9 kg of Boluo pods, extract by diafiltration with 0.5% sulfuric acid, then use lye to adjust the solution to a pH value of about 10 to precipitate, obtain a precipitate after filtration, dry the precipitate, and dissolve it with 90% ethanol Sulfuric acid solution was added to precipitate, filtered, and after the precipitate was dried, 167.4 g of the extract was returned, and the percentage of sanguinarine was 42.8% as measured by liquid phase.
[0041] (2) Take 1kg of motherwort medicinal material, extract twice with 10 times of water, and concentrate the combined water extract to about 1.10g / cm 3 , add an equivalent amount of 95% ethanol to carry out alcohol precipitation, recover the alcohol liquid and dry it to obtain 92.5g of Motherwort extract, and the stachydrine hydrochloride is 3.1% as measured by the liquid phase.
[0042] (3) Merge the extract of Boluohui and motherwort, add 168g of sodium citrate and 33g of sodium carboxymethylcellulose, mix and pack...
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