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Rod-like zinc oxide-based composite nanoparticle glass fiber filter element and preparation method thereof

A composite nanoparticle, zinc oxide-based technology, applied in chemical instruments and methods, separation methods, metal/metal oxide/metal hydroxide catalysts, etc., can solve the problem of reduced photocatalytic antibacterial activity, easy agglomeration of photocatalytic particles, Visible light utilization efficiency is small and other problems, to achieve the effect of improving the antibacterial and sterilizing effect, large specific surface area, and excellent photocatalytic antibacterial performance of air purification glass fiber filter element

Active Publication Date: 2021-08-10
YUNNAN HUAPU QUANTUM MATERIAL CO LTD +6
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Photocatalytic particles have good indoor air purification ability by using the photocatalytic mechanism, but using the combination of photocatalytic particles and glass fiber filter elements, most of the photocatalytic antibacterial inner filters are mechanically supported by photocatalytic particles. The photocatalyst has a low utilization efficiency of visible light, and the photocatalytic particles are easy to agglomerate, which all lead to the reduction of photocatalytic antibacterial activity.
Antibacterial particles of precious metals are mainly added to the air filter element of the prior art to improve its antibacterial effect, but the cost is high. Therefore, the purpose of the present invention is to use the air filter element and the composite photocatalytic particle precursor solution for organic combination to provide a kind of improved glass. The air purification rate of the fiber air filter element and the preparation method of the antibacterial air purification and glass fiber purification filter element of the fast visible light response that the photocatalyst is closely combined

Method used

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  • Rod-like zinc oxide-based composite nanoparticle glass fiber filter element and preparation method thereof
  • Rod-like zinc oxide-based composite nanoparticle glass fiber filter element and preparation method thereof
  • Rod-like zinc oxide-based composite nanoparticle glass fiber filter element and preparation method thereof

Examples

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Effect test

Embodiment 1

[0035] Weigh 2 g of zinc acetate and dissolve it in 50 ml of deionized water, add 1.5 ml of ammonia water, filter the precipitate and dry it at 45° C. for 10 h. Weigh the zinc ammonia complex, nano-silver wire, graphene oxide and nano-titanium oxide to form a rod-shaped zinc oxide solution precursor of 6 mol / l, wherein 20 ml of ammonia water and 20 ml of deionized water are used. Take 40 parts of ultra-fine glass fiber cotton with a diameter of 3.0 μm and 10 parts of ultra-fine glass fiber cotton with a diameter of 1.0 μm, and disintegrate the glass fiber cotton at a speed of 6000 rpm for 3 minutes through a fiber dissociator to prepare A pulp suspension with a mass concentration of 6%. It is transported by the slurry conveyor to the forming paper machine for wet forming and then made into sheets. Then soak the formed wet paper in the binder system mixed and diluted with polyurethane modified phenolic resin and KH550 to account for 3% by weight, and dry it on a drying plate a...

Embodiment 2

[0037]Weigh 3g of zinc sulfate and dissolve it in 50ml of deionized water, add 2ml of ammonia water, filter the precipitate and dry it at 45°C for 10h. Weigh the zinc ammonia complex, nano-silver wire, graphene oxide, and nano-titanium oxide to form a rod-shaped zinc oxide solution precursor of 7 mol / l, wherein 20 ml of ammonia water and 20 ml of deionized water are used. Take 40 parts of ultra-fine glass fiber cotton with a diameter of 3.5 μm and 10 parts of ultra-fine glass fiber cotton with a diameter of 1.5 μm, and disintegrate the glass fiber cotton at a speed of 7000 rpm for 4 minutes through a fiber dissociator to prepare A pulp suspension with a mass concentration of 7%. It is transported by the slurry conveyor to the forming paper machine for wet forming and then made into sheets. Then soak the molded wet paper in the binder system mixed and diluted with polyurethane modified phenolic resin and KH550 to account for 6% by weight, and dry it on a drying plate at 100°C ...

Embodiment 3

[0039] Weigh 4g of zinc acetate and dissolve it in 50ml of deionized water, add 3ml of ammonia water, filter the precipitate and dry it at 45°C for 10h. Weigh the zinc ammonia complex, nano-silver particles, graphene oxide, and nano-titanium oxide to form a rod-shaped zinc oxide solution precursor of 8 mol / l, wherein 20 ml of ammonia water and 20 ml of deionized water are used. Take 40 parts of ultra-fine glass fiber cotton with a diameter of 3.5 μm and 10 parts of ultra-fine glass fiber cotton with a diameter of 1.5 μm, and disintegrate the glass fiber cotton at a speed of 8000 rpm for 4 minutes through a fiber dissociator to prepare A pulp suspension with a mass concentration of 9%. It is transported by the slurry conveyor to the forming paper machine for wet forming and then made into sheets. Then soak the molded wet paper in the binder system mixed and diluted with polyurethane modified phenolic resin and KH550 to account for 6% by weight, and dry it on a drying plate at ...

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Abstract

The invention discloses a rod-like zinc oxide-based composite nanoparticle glass fiber filter element and a preparation method thereof. The photocatalytic air purification composite glass fiber filter element comprises the following components: 6-12wt% of rodlike zinc oxide-based composite photocatalytic nanoparticles, 3-9wt% of a bonding system and 79-91wt% of superfine glass fiber cotton. The invention also discloses a preparation method of the rod-like zinc oxide-based composite nanoparticle glass fiber filter element, which comprises the steps of firstly, preparing glass fiber filter paper by a wet papermaking process, and then completing in-situ growth through a microwave rapid reaction to introduce the rod-like zinc oxide-based composite photocatalytic nano-scale particles, then enabling the prepared glass fiber filter paper to be subjected to folding treatment, and obtaining the rod-like zinc oxide-based composite nanoparticle air purification glass fiber filter element with the visible light photocatalysis effect. The prepared material has a visible light catalysis antibacterial purification function and has a wide application prospect in the field of high-density air pollution purification.

Description

technical field [0001] The invention belongs to the technical field of composite functional materials, and in particular relates to a rod-shaped zinc oxide-based composite nanoparticle glass fiber filter element and a preparation method thereof. Background technique [0002] Photocatalytic particles have good indoor air purification ability by using the photocatalytic mechanism, but using the combination of photocatalytic particles and glass fiber filter elements, most of the photocatalytic antibacterial inner filters are mechanically supported by photocatalytic particles. The photocatalyst has a low utilization efficiency of visible light, and the photocatalytic particles are easy to agglomerate, which all lead to the reduction of photocatalytic antibacterial activity. Antibacterial particles of precious metals are mainly added to the air filter element of the prior art to improve its antibacterial effect, but the cost is high. Therefore, the purpose of the present inventio...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D39/20B01J23/66
CPCB01D39/2017B01D39/2027B01D39/20B01J23/66B01J35/19B01J35/39Y02W10/37
Inventor 曾和平翟福强胡梦云李璐罗永以冯光
Owner YUNNAN HUAPU QUANTUM MATERIAL CO LTD