The invention discloses carboxyl magnetic beads and a preparation method thereof, and relates to the technical field of
polymer synthesis, a
sodium hydroxide solution is prepared and added into a flask, deionized water is used for washing for 2-3 times,
vacuum drying is performed for standby application, a
suspension polymerization stabilizer and deionized water are added into the flask and stirred and dissolved at
room temperature, deionized water and ethyl
alcohol are used for washing products in sequence, and the carboxyl magnetic beads are obtained. Performing
vacuum drying on the Fe3O4 / PS microspheres for later use, preparing a deionized water /
ethanol solution, and adding the deionized water /
ethanol solution into a flask; according to the carboxyl magnetic beads and the preparation method thereof, the conversion rate is high, the particle size uniformity degree is high, carboxyl groups are grafted on the surfaces of the microspheres through free radical in-situ
polymerization reaction, the carboxyl magnetic beads have the characteristics of high carboxyl
grafting rate, uniform distribution and the like, the carboxyl magnetic beads are modified by N (3-aminopropyl)
methacrylamide, the steric hindrance among the carboxyl magnetic beads can be increased, and the stability of the magnetic beads is improved. Therefore,
dispersity and stability of carboxyl magnetic beads are improved,
chemical stability of the carboxyl magnetic beads is guaranteed, and oxidation is reduced.