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Preparation method of functionalized polyester fiber

A polyester fiber and functionalization technology, applied in the field of preparation of functionalized polyester fiber, can solve the problems of narrow applicability and complex processing technology, and achieve the effects of high universality, improvement of agglomeration phenomenon, and simple operation.

Active Publication Date: 2012-10-10
DONGHUA UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In CN101768258A, a kind of chemical method is provided to connect CBT catalyst on POSS nano material, and join in CBT, be used to prepare PBT / POSS novel nanocomposite material, this method makes POSS nano material become the active center of reaction, The dispersion of functional powders in the organic matrix has been further improved. However, the use of chemical methods to attach catalytic groups to nanomaterials requires certain requirements for materials, and the processing technology is also relatively complicated. The applicability of this method is relatively narrow. has certain limitations

Method used

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  • Preparation method of functionalized polyester fiber
  • Preparation method of functionalized polyester fiber
  • Preparation method of functionalized polyester fiber

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0046] (1) Preparation of PBT-coated carbon nanotube powder

[0047] 1) Carry a layer of CBT catalyst on the surface of carbon nanotube powder: dissolve the catalyst ethyl titanate in ethanol to form a solution with a mass concentration of 25%; add carbon nanotube powder to the above solution in, and stirred; the particle diameter of the carbon nanotube powder is 20nm, and the mass ratio of the carbon nanotube powder to the ethyl titanate in the solution is 15:1; standing for stratification, obtaining the lower layer of precipitation , further remove the ethanol solvent at 90°C to obtain the loaded carbon nanotube powder loaded with ethyl titanate, figure 1 It is a schematic diagram of a loaded functional powder with a CBT catalyst on its surface, that is, a schematic diagram of a loaded carbon nanotube powder with ethyl titanate loaded on its surface. The functional powder shown in Figure 1 is a carbon nanotube powder , 2 means that the titanium catalyst is ethyl titanate, c...

Embodiment 2

[0055] (1) Preparation of PBT-coated nano-titanium dioxide powder

[0056] 1) Carry a layer of CBT catalyst on the surface of nano-titanium dioxide powder: dissolve the catalyst isopropyl titanate in ethanol to form a solution with a mass concentration of 35%; add nano-titanium dioxide powder to the above solution , and stirred; the particle size of the nano-titanium dioxide powder is 40nm, and the mass ratio of the nano-titanium dioxide powder to the isopropyl titanate in the solution is 25:1; standing for stratification, obtaining the lower layer of precipitation, and The ethanol solvent is further removed at 100°C to obtain nano-sized titanium dioxide powder loaded with isopropyl titanate. figure 1 It is a schematic diagram of a loaded functional powder loaded with a CBT catalyst on the surface, that is, a schematic diagram of a loaded nano-titanium dioxide powder loaded with isopropyl titanate on the surface. The functional powder shown in Figure 1 is a nano-titanium dioxi...

Embodiment 3

[0074] (1) Preparation of PBT-coated tourmaline powder

[0075]1) Carry a layer of CBT catalyst on the surface of the tourmaline powder: dissolve the catalyst 2-ethylhexyl titanate in ethanol to form a solution with a mass concentration of 30%; add the tourmaline powder to in the above solution, and stirred; the particle diameter of the tourmaline powder is 60nm, and the mass ratio of the tourmaline powder to the 2-ethylhexyl titanate in the solution is 20:1; , to obtain the lower precipitate, and further remove the ethanol solvent at 95°C to obtain the loaded tourmaline powder loaded with 2-ethylhexyl titanate, figure 1 It is a schematic diagram of a loaded functional powder with a CBT catalyst loaded on its surface, that is, a schematic diagram of a loaded tourmaline powder with 2-ethylhexyl titanate loaded on its surface. The functional powder shown in Figure 1 is tourmaline Powder, the titanium catalyst represented by 2 is 2-ethylhexyl titanate. After the tourmaline powde...

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Abstract

The invention relates to a preparation method of a functionalized polyester fiber. The functionalized polyester fiber is prepared through blended spinning of functional powder coated by polyester chips and polybutylece terephthalate (PBT). A preparation method of the functional powder coated by the PBT includes that a layer of titanium catalysts is supported on the surface of the functional powder, added polybutylece terephthalate cyclic oligomer (CBT) polymerizes on the surface of the functional powder and generates PBT resin under the action of the catalysts, and the functional powder coated by the PBT is obtained after spray powdering. The catalysts for the polymerization of the CBT are supported on the surface of the functional powder through a supporting technology, the mass ratio of the PBT resin to the functional powder is (2-4):1, the mass ratio of the polyester chips to the functional powder coated by the PBT is (10-15):1, the functional powder coated by the PBT has a good compatibility with polyester, and the functionalized effects of the obtained functionalized polyester fiber are excellent.

Description

technical field [0001] The invention relates to the field of functional materials, in particular to a preparation method of functionalized polyester fibers. Background technique [0002] With the continuous development of the fiber industry, people's requirements for fibers are not limited to the functions of covering the body and beauty in the past, but more focus on realizing the functionalization and diversified use of fibers. At present, the functional modification of various synthetic fibers including polyester fiber and polyamide fiber has made great progress. The main functional means include chemical grafting of fibers, blend spinning and fabric modification. Finishing method, etc., wherein the functionalization of fibers by blend spinning method is the easiest and most effective means, and the functionalization effect of the obtained fibers is also relatively long-lasting. Most of the functional powders used in the fiber functionalization process are inorganic mate...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01F6/92D01F1/10
Inventor 王彪李莉王华平
Owner DONGHUA UNIV
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