TPE (Thermoplastic Elastomer) gasket material for resisting content migration as well as preparation and processing methods of TPE gasket material
A content and gasket technology, which is applied to the TPE gasket material that resists content migration and its preparation and processing, can solve the problems of reducing the overall mechanical properties and structural strength, changing the structural shape of TPE thermoplastic elastomers, etc., and achieving improvement Effect of content migration resistance, excellent mechanical properties and processing fluidity, and balanced properties
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preparation example 1
[0051] Matrix preparation: Add 0.1kg of accelerator TETD and 1kg of zinc stearate to 40kg of olefin block copolymer, stir and mix and place at 200°C for mastication for 15 minutes to collect the mastication matrix glue;
[0052] Compatibility modification: Stir and mix 5 kg of molten poly-4-methylpentene-1 particles and 30 kg of plasticized base rubber and place it in a torque rheometer at 100°C, stir and mix, heat-preserve and vulcanize, collect the vulcanized rubber and open Refining treatment, standing still and then crushing through a 200-mesh sieve to prepare modified rubber elastomer 1.
preparation example 2
[0054] Matrix preparation: Add 0.1kg of accelerator TETD and 1kg of zinc stearate to 45kg of olefin block copolymer, stir and mix and place it at 200°C for 17.5 minutes of mastication treatment, and collect the mastication matrix glue;
[0055] Compatibility modification: Stir and mix 5 kg of molten poly-4-methylpentene-1 particles and 35 kg of plasticizing base rubber and place it in a torque rheometer at 105°C, stir and mix, heat-preserve and vulcanize, collect the vulcanized rubber and open Refining treatment, standing still and then crushing through a 200-mesh sieve to prepare modified rubber elastomer 2.
preparation example 3
[0057] Matrix preparation: Add 0.1kg of accelerator TETD and 1kg of zinc stearate to 50kg of olefin block copolymer, stir and mix and masticate at 200°C for 20 minutes to collect the plasticized matrix glue;
[0058] Compatibility modification: Stir and mix 5kg of melted poly-4-methylpentene-1 particles and 40kg of plasticized base rubber and place it in a torque rheometer at 110°C, stir and mix, heat-preserve and vulcanize, collect the vulcanized rubber and open Refining treatment, standing and parking, and crushing through a 200-mesh sieve to prepare modified rubber elastomer 3.
[0059] performance test
[0060] The modified rubber elastomers prepared in Preparation Examples 1 to 3 and the olefin block copolymers with equal mass were used as blank groups, and thermal performance tests were carried out.
[0061] Detection method / test method
[0062] Thermal properties: Characterized by a thermogravimetric analyzer (heating rate 20 K / min, nitrogen atmosphere), the specific ...
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