High-thermal-conductivity semi-cured adhesive film of metal substrate and preparation method of high-thermal-conductivity semi-cured adhesive film
A metal substrate, semi-curing technology, used in adhesives, epoxy resins, film/sheet adhesives, etc., can solve the problems of easy embrittlement, easy tearing, accelerated embrittlement, etc. Thermal conductivity, strong crosslinking, effect of improving thermal conductivity and toughness
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Embodiment 1
[0041] A high thermal conductivity prepreg film for a metal substrate, calculated in parts by weight, includes the following parts by weight:
[0042] 100 parts of epoxy resin, 20 parts of thermally conductive filler, 35 parts of curing agent and 6 parts of curing agent accelerator;
[0043] Wherein, the thermally conductive filler is modified boron nitride / tantalum disilicide microspheres.
[0044] Described epoxy resin is the mixture of bisphenol A type epoxy resin, naphthalene ring epoxy resin and biphenyl epoxy resin, the weight ratio of bisphenol A type epoxy resin, naphthalene ring epoxy resin and biphenyl epoxy resin 30:8:15.
[0045] The curing agent is methyl tetrahydrophthalic anhydride.
[0046] The curing agent accelerator is 2,4,6-tris(dimethylaminomethyl)phenol.
[0047] The thermally conductive filler is treated boron nitride, and the treatment method of boron nitride is:
[0048] Step 1, treating boron nitride with acid solution, and then grafting with zinc...
Embodiment 2
[0067] A high thermal conductivity prepreg film for a metal substrate, calculated in parts by weight, includes the following parts by weight:
[0068] 100 parts of epoxy resin, 16 parts of thermally conductive filler, 20 parts of curing agent and 3 parts of curing agent accelerator;
[0069] Wherein, the thermally conductive filler is modified boron nitride / tantalum disilicide microspheres.
[0070] Described epoxy resin is the mixture of bisphenol A type epoxy resin, naphthalene ring epoxy resin and biphenyl epoxy resin, the weight ratio of bisphenol A type epoxy resin, naphthalene ring epoxy resin and biphenyl epoxy resin It is 25:5:10.
[0071] The curing agent is dimer acid-based polyamide.
[0072] The curing agent accelerator is N,N-dimethylbenzylamine.
[0073] The thermally conductive filler is treated boron nitride, and the treatment method of boron nitride is:
[0074] Step 1, treating boron nitride with acid solution, and then grafting with zinc phenolsulfonate ...
Embodiment 3
[0094] A high thermal conductivity prepreg film for a metal substrate, calculated in parts by weight, includes the following parts by weight:
[0095]100 parts of epoxy resin, 24 parts of thermally conductive filler, 50 parts of curing agent and 9 parts of curing agent accelerator;
[0096] Wherein, the thermally conductive filler is modified boron nitride / tantalum disilicide microspheres.
[0097] Described epoxy resin is the mixture of bisphenol A type epoxy resin, naphthalene ring epoxy resin and biphenyl epoxy resin, the weight ratio of bisphenol A type epoxy resin, naphthalene ring epoxy resin and biphenyl epoxy resin It is 45:10:20.
[0098] The curing agent is 4,4-diaminodiphenyl sulfone.
[0099] The curing agent accelerator is N,N-dimethylbenzylamine.
[0100] The thermally conductive filler is treated boron nitride, and the treatment method of boron nitride is:
[0101] Step 1, treating boron nitride with acid solution, and then grafting with zinc phenolsulfonate...
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