A kind of intelligent atomized glass with low driving voltage and preparation process thereof
A low driving voltage, atomized glass technology, applied in the fields of instruments, optics, nonlinear optics, etc., can solve the problem of high working voltage of dimming glass, reduce driving voltage and power consumption, increase load rate, and reduce excessive moisture content high effect
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preparation example 1
[0062] S1, blending, specifically,
[0063] Graphene oxide was dissolved in deionized water for ultrasonic dispersion, and 1.2 g of graphene oxide was added per 1 L of deionized water. The ultrasonic power is 300W, and the ultrasonic time is 30min. After the ultrasonication is completed, centrifuge at a speed of 7000rmp. After centrifugation, the supernatant is taken, and nitrogen gas is injected for 30min to remove the oxygen in the solution, and the graphene oxide solution is obtained for use.
[0064] Dissolve ferrous chloride tetrahydrate and ferric chloride hexahydrate in deionized water, add 0.15mol of ferrous chloride tetrahydrate and 0.2mol of ferric chloride hexahydrate for every 1L of deionized water, and stir to make the solid completely Dissolve, and then blow nitrogen into the solution for 30 minutes to remove the oxygen in the solution to obtain the iron ion solution.
[0065] Under the protection of nitrogen atmosphere, put the iron ion solution into the graphe...
preparation example 2
[0069] The difference between Preparation Example 2 and Preparation Example 1 is that the specific process of step S2 is different, and specifically includes the following steps:
[0070] S21. Primary deposition. Slowly add ammonia water dropwise to the mixed liquid obtained in step S1 until the pH of the system is 9. Incubate and deposit at a temperature of 70° C. for 1 hour, keep stirring at a stirring speed of 200 rpm to obtain a primary deposition liquid.
[0071] S22. Secondary deposition. Continue to add ammonia water dropwise to the primary deposition solution obtained in step S21 until the pH of the system is 10.5, and keep stirring for 1 hour to obtain the deposition solution.
preparation example 3
[0073] The difference between Preparation Example 3 and Preparation Example 2 is that in step S21, aqueous ammonia is added dropwise until the pH of the system is 9.5; in step S22, aqueous ammonia is added dropwise until the pH of the system is 11.
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