Preparation method of cod skin collagen peptide copper chelate
A technology of copper chelate and skin collagen is applied in the field of preparation of cod skin collagen peptide copper chelate, which can solve the problems of rare peptide chelating copper ions and the like, achieve good economic and social benefits, less environmental pollution, The effect of promoting development
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Embodiment 1
[0018] A method of preparation of a cod pulverut protein peptide copper chelate, including the following steps:
[0019] (1) Weigh a certain amount of squid skin collagen peptide and copper, placed in a beaker, add 100 ml of distilled water, thoroughly mixed, and heat the water bath.
[0020] (2) After sufficient reactions, add an appropriate amount of water-absorbent ethanol, filtrate, dried down 100 ° C water vapor to dry, with a mortar to abrasive the product, over 60 mesh sieve, weigh;
[0021] (3) Weigh EDTA3.7224G, dissolve with hot water, dilute to 500 ml, and stand after 24 to 48 hours;
[0022] (4) 0.2gpan is dissolved in ethanol, diluted with ethanol to 100 m;
[0023] (5) Weigh 8 g of a cod collagen peptide powder with 2 g of copper powder, fixed reaction temperature 50 ° C, reactive 30min, control pH 712, set each pH as a reaction control unit, each unit reaction is completed, Maximum absorbance wavelength under test;
[0024] (6) Weigh 8 g of a squid skin collagen pep...
Embodiment 2
[0027] A method of preparation of a cod pulverut protein peptide copper chelate, including the following steps:
[0028] (1) Weigh a certain amount of squid skin collagen peptide and copper, placed in a beaker, add 100 ml of distilled water, thoroughly mixed, and heat the water bath.
[0029] (2) After sufficient reactions, add an appropriate amount of water-absorbent ethanol, filtrate, dried down 100 ° C water vapor to dry, with a mortar to abrasive the product, over 60 mesh sieve, weigh;
[0030] (3) Weigh EDTA3.7224G, dissolve with hot water, dilute to 500 ml, and stand after 24 to 48 hours;
[0031] (4) 0.2gpan is dissolved in ethanol, diluted with ethanol to 100 m;
[0032] (5) Weigh 8 g of a cod collagen peptide powder with 2 g of copper powder, fixed reaction temperature 50 ° C, reactive 30min, control pH 712, set each pH as a reaction control unit, each unit reaction is completed, Maximum absorbance wavelength under test;
[0033] (6) Weigh 8 g of a squid skin collagen pep...
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