Tough particle plugging system for fractured leakage well drilling plugging and preparation method thereof
A ductile and granular technology, which is applied in the field of ductile particle plugging system and its preparation for fractured leakage drilling and plugging, can solve problems such as difficulty in predicting the opening degree of lost fractures, unsatisfactory effect of plugging while drilling, and wellbore scrapping.
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Embodiment 1
[0019] In the indoor environment, the specific gravity of 10g is 0.82g / cm 3 , tensile modulus 3.0 MPa, tensile strength 8.0 MPa, elongation 500%, flexural modulus 10.0, softening temperature 40°C, oval tough particles with a particle size of 2mm, weigh 5g isooctyl phosphate, dissolve in 200mL of water, fully stirred, under the condition of 50 ℃, the tough particles were dispersed in isooctyl phosphate, stirred and aged for 30min, taken out, and dried at low temperature to obtain isooctyl phosphate modified particles.
[0020] In 1000mL water, add 50g sodium carboxymethylcellulose, 20g bistriethanolamine diisopropyl titanate, 30g sodium laurate, 20g sodium dodecylsulfonate, 20g sodium metaaluminate, 10g sodium bicarbonate, Fully stir under the high-speed mixer not lower than 600r / min to form a recyclable foam carrying system.
[0021] Add the obtained isooctyl phosphate-modified particles into 1000mL liquid system, and mix well to form the required tough particle plugging syst...
Embodiment 2
[0029] In the indoor environment, the specific gravity of 10g is 0.82g / cm 3 , tensile modulus 3.0 MPa, tensile strength 8.0 MPa, elongation 500%, flexural modulus 10.0, softening temperature 40 ℃. For round tough granules with a particle size of 1mm, weigh 5g of phosphate starch, dissolve it in 200mL of water, stir thoroughly, and disperse the tough granules in phosphate starch at 50°C, stir and age for 30min, take it out, dry it at low temperature, and set aside .
[0030] In 1000mL water, add 50g sodium carboxymethylcellulose, 60g polyacrylamide, 20g bistriethanolamine diisopropyl titanate, 30g sodium carboxyethylcellulose, 20g sodium dodecylbenzenesulfonate, 10g carbonic acid Sodium, fully stirred with a high-speed mixer not lower than 600r / min to form a recyclable foam carrying system.
[0031] Add phosphate starch surface-modified granules into 1000mL liquid system, and mix well to form the required tough granule plugging system.
[0032] As mentioned above, the indoor...
Embodiment 3
[0034] In the indoor environment, the specific gravity of 10g is 0.79g / cm 3 , tensile modulus 4.0 MPa, tensile strength 10.0 MPa, elongation 650%, flexural modulus 12.0, softening temperature 45 ℃. For clover-shaped tough particles with a particle size of 3mm, weigh 5g of dodecyl phosphate, dissolve it in 200mL of water, stir well, and disperse the tough particles in the aqueous solution of dodecyl phosphate at 50°C, stir and age for 30min. Take it out, dry it on low temperature, and set aside.
[0035] In 1000mL water, add 50g sodium carboxymethylcellulose, 40g carboxyethylcellulose, 25g xanthan gum, 30g sodium carboxyethylcellulose, 20g sodium lauryl sulfate, 10g triethanolamine, 10g sodium bicarbonate, Fully stir under the high-speed mixer not lower than 600r / min to form a recyclable foam carrying system.
[0036] Add phosphate starch surface-modified granules into 1000mL liquid system, and mix well to form the required tough granule plugging system.
[0037] As mentione...
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