Plant-based antioxidant composition and application thereof
An antioxidant, plant-based technology, applied in the field of plant-derived natural antioxidants, can solve the problems of animal body toxicity, carcinogenic risk, volatile and other problems
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Embodiment 1
[0035] The jujube leaves of Jujube jujuba in Linxian County, Luliang, Shanxi are picked, dried, and crushed into jujube leaf meal.
[0036] Weigh 500g of jujube leaf coarse powder, add 5L of deionized water heated to 90°C, soak in heat for 10h, continue to reflux extraction at this temperature for 1h, let it stand, and separate the extract and solid residue.
[0037] Filter the extract with a hollow fiber ultrafiltration membrane with a molecular weight cut-off of less than 150,000, and collect the filtrate.
[0038] Add 5 L of deionized water to the solid residue, raise the temperature to 90° C. for reflux extraction for 1 h, and collect the filtrate in the same way.
[0039] Combine the two filtrates, keep the vacuum degree of -0.1~-0.08MPa on the rotary evaporator, and concentrate under reduced pressure to 50ml by distillation at 65°C while maintaining a slight boiling state, and prepare jujube leaves with a final concentration equivalent to about 10g of raw materials / ml E...
Embodiment 2
[0044] The jujube leaves of Xinjiang Junzao are picked, dried, and crushed into jujube leaf powder.
[0045] Weigh 500g of jujube leaf coarse powder, add 5L of deionized water to soak for 12h, heat to reflux temperature and extract for 2h, filter with fast filter paper, and collect the filtrate.
[0046] 5 L of deionized water was added to the solid residue, heated to reflux temperature for extraction for 2 h, and the filtrate was collected by rapid filter paper filtration.
[0047] Combine the 2 filtrates, centrifuge at a speed of 2000 rpm for 10 min in a centrifuge, take the supernatant, maintain a vacuum degree of -0.1 to -0.08 MPa on a rotary evaporator, concentrate under reduced pressure at 70 ° C to 50 ml, and prepare a final concentration of approximately It is the jujube leaf extract concentrate equivalent to 10g raw material / ml.
[0048] Weigh 500g of seabuckthorn leaf coarse powder, and prepare a seabuckthorn leaf extract concentrate with a final concentration appro...
Embodiment 3
[0051] Extract the jujube leaves of Cangzhou Jinsixiaozao in Hebei, dry them, and grind them into coarse powder of jujube leaves.
[0052] Weigh 500g of jujube leaf coarse powder, add 5L of deionized water to soak for 12h, extract in a microwave oven with a power of 300W for 30min, filter with fast filter paper, and collect the filtrate.
[0053] Add 5 L of deionized water to the solid residue, extract in a microwave oven at 300W for 30 min, filter through fast filter paper and collect the filtrate.
[0054] Combine the 2 filtrates, centrifuge at a speed of 2000 rpm for 10 min in a centrifuge, take the supernatant, maintain a vacuum degree of -0.1 to -0.08 MPa on a rotary evaporator, concentrate under reduced pressure at 70 ° C to 50 ml, and prepare a final concentration of approximately It is the jujube leaf extract concentrate equivalent to 10g raw material / ml.
[0055] Weigh 500g of seabuckthorn leaf coarse powder, and prepare a seabuckthorn leaf extract concentrate with a...
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